Type	HazMat fee for 500 gram (Estimated)
Excepted Quantity	USD 0.00
Limited Quantity	USD 15-60
Inaccessible (Haz class 6.1), Domestic	USD 80+
Inaccessible (Haz class 6.1), International	USD 150+
Accessible (Haz class 3, 4, 5 or 8), Domestic	USD 100+
Accessible (Haz class 3, 4, 5 or 8), International	USD 200+

CAS No. :	1195529-07-7
Formula :	C₁₇H₁₁NO₄
M.W :	293.27
SMILES Code :	O=C(ON(C(C1=C2C=CC=C1)=O)C2=O)/C=C/C3=CC=CC=C3
English Name :	1,3-Dioxoisoindolin-2-yl cinnamate
MDL No. :	MFCD00405209
InChI Key :	RWBPSIPMHURWQQ-ZHACJKMWSA-N
Pubchem ID :	6008258

GHS Pictogram:
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Yield	Reaction Conditions	Operation in experiment
89%	With dmap; dicyclohexyl-carbodiimide In 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran at 20℃; for 2h; Schlenk technique; Inert atmosphere;
87%	With dmap; dicyclohexyl-carbodiimide In tetrahydrofuran at 20℃; for 15h;
68%	With triethylamine In 2-methyltetrahydrofuran; ethyl acetate at 60℃; for 24h; Sealed tube; Green chemistry;	General procedure for the preparation of N-(acyloxy)phthalimides (1). General procedure: In a sealed vial, N-hydroxyphthalimide (13, 2.0 mmol) or N-hydroxy compounds (15, 2.0 mmol), the corresponding carboxylic acid (14, 2.0 mmol), T3P (50% in EtOAc, 1.41 mL, 2.4 mmol, 1.2 equiv.) and triethylamine (0.333 mL, 2.4 mmol, 1.2 equiv.) were dissolved in 2-Me-THF (10 mL). The mixture was stirred at room temperature or at 60 °C for 2448 h. After the reaction was complete (followed by TLC, hexaneEtOAc 4:1), 2-Me-THF (50 mL) was added to the mixture and the organic phase was extracted with a 5% NaHCO3 solution (50 mL) and washed with distilled water (50 mL). The organic layer was dried over Na2SO4 and after filtration, the volatiles were evaporated. Analytical samples were purified by recrystallization from the solvent given below after the melting point. Compounds 1am, 1q, 1t and 17a are known from the literature, while 1np, 1r, 1s and 17b are new substances

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P222	Do not allow contact with air.
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P230	Keep wetted
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P232	Protect from moisture.
P233	Keep container tightly closed.
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Code	Phrase
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P337 + P313	IF eye irritation persists: Get medical advice/attention.
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P401
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CAS No.: 1195529-07-7

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CAS No.: 1195529-07-7

Alternative Products

Product Details of [ 1195529-07-7 ]

Safety of [ 1195529-07-7 ]

Application In Synthesis of [ 1195529-07-7 ]

[ 1195529-07-7 ] Synthesis Path-Downstream 1~7

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Physical hazards
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H200	Unstable explosive
H201	Explosive; mass explosion hazard
H202	Explosive; severe projection hazard
H203	Explosive; fire, blast or projection hazard
H204	Fire or projection hazard
H205	May mass explode in fire
H220	Extremely flammable gas
H221	Flammable gas
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H225	Highly flammable liquid and vapour
H226	Flammable liquid and vapour
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H231	May react explosively even in the absence of air at elevated pressure and/or temperature
H240	Heating may cause an explosion
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H242	Heating may cause a fire
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H251	Self-heating; may catch fire
H252	Self-heating in large quantities; may catch fire
H260	In contact with water releases flammable gases which may ignite spontaneously
H261	In contact with water releases flammable gas
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H290	May be corrosive to metals
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Code	Phrase
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H302	Harmful if swallowed
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