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Chemical Structure| 1197956-03-8 Chemical Structure| 1197956-03-8

Structure of 1197956-03-8

Chemical Structure| 1197956-03-8

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Product Details of [ 1197956-03-8 ]

CAS No. :1197956-03-8
Formula : C9H14NO2P
M.W : 199.19
SMILES Code : CP(C)(C1=CC=C(C(OC)=C1)N)=O
MDL No. :MFCD30303983
InChI Key :XSUFWLZYYKQQRC-UHFFFAOYSA-N
Pubchem ID :67052699

Safety of [ 1197956-03-8 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H312-H315-H319-H332-H335
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 1197956-03-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1197956-03-8 ]

[ 1197956-03-8 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 76661-24-0 ]
  • [ 1197956-03-8 ]
  • [ 1407520-09-5 ]
YieldReaction ConditionsOperation in experiment
58% With potassium phosphate; palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In N,N-dimethyl-formamide; at 120℃;Sealed tube; Compound 19 (154mg, 0.54mmol) and compound 20 (107mg, 0.54mmol) were dissolved in 4 mL anhydrous DMF in a sealed tube and was added Pd(OAc)2 (14mg, 0.062mmol), XantPhos (37mg, 0.064mmol), and K3PO4 (150mg, 0.71 mmol). The content was heated at 120 C overnight. After cooling to the room temp, EtOAc was added and the mixture was filtered through celite, washed with more EtOAc. Combined filtrate was cone in vacuo, and the residue was purified by CombiFlash (MeOH/DCM). The product 21 (140 mg, yield 58%) was obtained as an orange solid.
  • 2
  • [ 1197956-03-8 ]
  • [ 1197953-49-3 ]
  • (2-((5-chloro-2-((4-(dimethylphosphoryl)-2-methoxyphenyl)amino)pyrimidin-4-yl)amino)phenyl)dimethylphosphine oxide [ No CAS ]
 

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