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CAS No. : | 1202-66-0 | MDL No. : | MFCD01670887 |
Formula : | C10H13NO2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | ATDWJOOPFDQZNK-UHFFFAOYSA-N |
M.W : | 179.22 | Pubchem ID : | 121051 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H319 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
86% | With sodium hydrogencarbonate In tetrahydrofuran; water | GK3-015 was prepared according to the following reaction scheme 12 |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
99% | at 90℃; for 24 h; Inert atmosphere | General procedure: To a solution of tBuCO2H (3d) (30.9 mg, 0.30 mmol) in EtOAc (3.0 mL) at room rtemperature was added 3-amino-1-phenylbutane (1) (48.7 μL, 0.30 mmol). The reaction mixture was refluxed (90 °C) for 24 h and then it was evaporated the solvent. The crude product was purified preparative thin layer chromatography on silica (hexane/EtOAc/35percent NH3 = 25/75/1) to afford the corresponding acetoamide 2 (57.0 mg, 99percent yield) as a colorless oil. |
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