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[ CAS No. 1210-66-8 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 1210-66-8
Chemical Structure| 1210-66-8
Structure of 1210-66-8 * Storage: {[proInfo.prStorage]}
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Product Details of [ 1210-66-8 ]

CAS No. :1210-66-8 MDL No. :MFCD04457455
Formula : C11H9N5 Boiling Point : -
Linear Structure Formula :- InChI Key :WCZNSRQVTJYMRQ-UHFFFAOYSA-N
M.W : 211.22 Pubchem ID :71029
Synonyms :

Safety of [ 1210-66-8 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P305+P351+P338 UN#:N/A
Hazard Statements:H315-H319 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 1210-66-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1210-66-8 ]

[ 1210-66-8 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 59278-00-1 ]
  • [ 1210-66-8 ]
  • 9-[(2-acetoxyethoxy)methyl]-6-phenylaminopurine [ No CAS ]
  • 4
  • [ 1210-66-8 ]
  • [ 15397-15-6 ]
  • 9-(2'-C-methyl-β-D-ribofuranosyl)-N6-phenyladenine [ No CAS ]
YieldReaction ConditionsOperation in experiment
75% Example 79; Synthesis of 2'-C-methyl-ss-D-ribofuranosyl-6-phenyladenine (155); 6-Phenyl-adenine (315 mg, 1.5 mmol) was suspended in 20 mL of dry CH3CN, BSA was added (0.4 mL) and the mixture was refluxed until the clear solution was formed (about 30 min). 1,2, 3, 5-Tetra-O-benzoyl-2'-C-methyl p-D- ribofuranose was added followed by trimethylsilyl trifluoromethane sulfonate (0.2 mL). The mixture was refluxed for 4 hours, disappearance of the sugar was controlled by TLC in hexane-ethyl acetate (1: 1 v/v). Solution of 10% NaHC03 was added and the benzoylated nucleoside was extracted with ethyl acetate. Water fraction was extracted with organic (2 x 30 mL). Combined organic fractions were washed with water, dried over Na2S04 and evaporated. The residue was dissolved in 20 mL of NH3/methanol and left overnight at ambient temperature. The reaction mixture was concentrated and purified by column chromatography on silica gel using ethyl acetate/iso-propanol/water (9: 1: 2, upper phase) as eluent. The title nucleoside was dissolved in methanol and precipitated with ether with 75% yield.
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