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Structure of 1213667-87-8

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Quality Control of [ 1213667-87-8 ] Purity: 95% SDS Specification

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Product Details of [ 1213667-87-8 ]

CAS No. :	1213667-87-8
Formula :	C₁₆H₂₇NO
M.W :	249.39
SMILES Code :	OC[C@H](C1=CC(C(C)(C)C)=CC(C(C)(C)C)=C1)N
English Name :	(S)-2-Amino-2-(3,5-di-tert-butylphenyl)ethanol
MDL No. :	MFCD09253894
InChI Key :	GODKSIZLEOJZHJ-CQSZACIVSA-N
Pubchem ID :	66515500

Safety of [ 1213667-87-8 ]

GHS Pictogram:
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Hazard Statements:
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Application In Synthesis of [ 1213667-87-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 1213667-87-8 ]

[ 1213667-87-8 ] Synthesis Path-Downstream 1~14

1
[ 1213667-87-8 ]
[ 10344-69-1 ]
[ 1251472-24-8 ]

Yield	Reaction Conditions	Operation in experiment
75%	In dichloromethane for 72h; Reflux;
49%	In tetrahydrofuran at 50℃; for 60h; Inert atmosphere; Sealed tube;
	In tetrahydrofuran at 50℃; for 48h; Inert atmosphere; Sealed tube;

	In dichloromethane Sealed tube;
	In dichloromethane Reflux;

References: [1]Li, Tao; Xu, Zhen; Huang, Yongliang; Zu, Weisai; Huo, Haohua [Journal of the American Chemical Society, 2025, vol. 147, # 13, p. 10999 - 11009].
[2]Tong, Xiaoyu; Schneck, Felix; Fu, Gregory C. [Journal of the American Chemical Society, 2022, vol. 144, # 32, p. 14856 - 14863].
[3]Zuo, Zhiwei; Cong, Huan; Li, Wei; Choi, Junwon; Fu, Gregory C.; MacMillan, David W. C. [Journal of the American Chemical Society, 2016, vol. 138, # 6, p. 1832 - 1835].
[4]Li, Shu-Sen; Sun, Shuo; Wang, Jianbo [Angewandte Chemie - International Edition, 2022, vol. 61, # 6][Angew. Chem., 2022, vol. 134, # 6].
[5]Liu, Xian-Ming; Li, Fu; Wang, Tongkun; Dai, Ling; Yang, Yin; Jiang, Neng-Quan; Xue, Li-Yuan; Liu, Jing-Yuan; Xue, Xiao-Song; Xiao, Li-Jun; Zhou, Qi-Lin [Journal of the American Chemical Society, 2025, vol. 147, # 1, p. 627 - 635].

2
[ 1872424-70-8 ]
[ 1213667-87-8 ]

Yield	Reaction Conditions	Operation in experiment
	Multi-step reaction with 4 steps 1: hydrogenchloride; methanol / 1,4-dioxane / 1 h / 20 °C 2: dmap; triethylamine / dichloromethane / 4 h / 20 °C 3: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere 4: water; potassium hydroxide; methanol / 14 h / 75 °C / Inert atmosphere
	Multi-step reaction with 2 steps 1: hydrogenchloride / methanol; 1,4-dioxane / 1 h / 0 - 20 °C 2: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere

References: [1]Zuo, Zhiwei; Cong, Huan; Li, Wei; Choi, Junwon; Fu, Gregory C.; MacMillan, David W. C. [Journal of the American Chemical Society, 2016, vol. 138, # 6, p. 1832 - 1835].
[2]Li, Qigang; Zhang, Mingkai; Zhan, Shuming; Gu, Zhenhua [Organic Letters, 2019, vol. 21, # 16, p. 6374 - 6377].

3
[ 22385-77-9 ]
[ 1213667-87-8 ]