Home Cart Sign in  
Chemical Structure| 1222010-52-7 Chemical Structure| 1222010-52-7

Structure of 1222010-52-7

Chemical Structure| 1222010-52-7

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 1222010-52-7 ]

CAS No. :1222010-52-7
Formula : C14H12BNO4
M.W : 269.06
SMILES Code : O=C(NC1=CC=CC=C1)OC2=CC3=C(C=C2)COB3O

Safety of [ 1222010-52-7 ]

Application In Synthesis of [ 1222010-52-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1222010-52-7 ]

[ 1222010-52-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1196473-37-6 ]
  • [ 103-71-9 ]
  • [ 1222010-52-7 ]
YieldReaction ConditionsOperation in experiment
18% 6-Hydroxyl-l,3-dihydro-l-hydroxy-2,l-benzoxaborole (0.667mmol) was dissolved in DMF (1OmL) and cooled to 00C with ice bath. To this solution under nitrogen were added in sequence triethylamine (0.28ml, 2mmol, 3.0eq) and isocyanatobenzene (0.852mL, 6.67mmol, lO.Oeq). The reaction mixture was stirred for 2 days at room temperature then treated with IM HCl (10ml). After extraction with ethyl acetate, the organic layer was washed with water and brine. The residue after rotary evaporation was purified by column chromatography over silica gel to give the title compound (32mg, 18percent yield). 1H NMR (300 MHz, DMSO-d6): delta 10.23 (s, IH), 9.25 (s, IH), 7.53-7.02 (m, 8H) and 5.00 (s, 2H) ppm.
 

Historical Records

Categories