Home Cart Sign in  
Chemical Structure| 1226795-80-7 Chemical Structure| 1226795-80-7

Structure of 1226795-80-7

Chemical Structure| 1226795-80-7

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 1226795-80-7 ]

CAS No. :1226795-80-7
Formula : C6H12N2
M.W : 112.17
SMILES Code : CC(N)C(C)(C)C#N
MDL No. :MFCD24445684

Safety of [ 1226795-80-7 ]

Application In Synthesis of [ 1226795-80-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1226795-80-7 ]

[ 1226795-80-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 37719-02-1 ]
  • [ 1226795-80-7 ]
YieldReaction ConditionsOperation in experiment
6% Step 3To a solution of <strong>[37719-02-1]2,2-dimethyl-3-oxo-butyronitrile</strong> (0.52 g, 4.72 mmol) in MeOH (10 mL) was added ammonium acetate (3.64 g, 47.2 mmol) and NaCNBH3 (0.296 g, 4.72 mmol). The reaction mixture was stirred at room temperature for 5 days then cooled to 0C and slowly treated with cone. HC1 until pH = 2 and stirred for 15 min at room temperature. The reaction mixture was concentrated and the residue was diluted with water and extracted with CH2CI2.The aqueous layer was made basic (pH = 10) with cone. NH4OH then extracted with CH2CI2. The organic layer was dried over MgS04 and concentrated to afford 0.031 g (6%) of 3- amino-2,2-dimethyl-butyronitrile as an oil.
 

Historical Records