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Chemical Structure| 123665-42-9 Chemical Structure| 123665-42-9

Structure of 123665-42-9

Chemical Structure| 123665-42-9

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Product Details of [ 123665-42-9 ]

CAS No. :123665-42-9
Formula : C11H17ClN2O
M.W : 228.72
SMILES Code : O=C(N(C)C)[C@@H](N)CC1=CC=CC=C1.[H]Cl

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Application In Synthesis of [ 123665-42-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 123665-42-9 ]

[ 123665-42-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 10241-97-1 ]
  • [ 123665-42-9 ]
  • [ 186430-35-3 ]
YieldReaction ConditionsOperation in experiment
Example 73 5-Methyl-1H-indole-2-carboxylic acid ((1S)-dimethylcarbamoyl-2-phenyl-ethyl)-amide (S)-2-Amino-N,N-dimethyl-3-phenyl-propionamide hydrochloride (1.0 mmol) and <strong>[10241-97-1]5-methyl-1H-indole-2-carboxylic acid</strong> (1.0 mmol) were coupled according to Procedure A (0 - 25 °C reaction temperature). The crude product was triturated with 1:1 ether-hexanes and dried. Yield 302 mg, 87 percent; HPLC (60/40) 5.46 minutes (99 percent); mp 198.5 - 200 °C; PBMS 350 (MH+, 100 percent); Anal. Calcd for C21H23N3O2: C, 72.18; H, 6.63; N, 12.04. Found: C, 72,14; H, 6.90; N, 12.11.
 

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