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CAS No. : | 1236861-77-0 | MDL No. : | MFCD28401439 |
Formula : | C13H22N2O3 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 254.33 | Pubchem ID : | - |
Synonyms : |
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Precautionary Statements: | UN#: | ||
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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
for 45h;Reflux; | A solution of C56 (20.6 g, 0.103 mol) in DMF dimethyl acetal was heated at reflux for 45 h. The reaction mixture was evaporated and azeotroped with toluene (2*200 mL) to afford C57, which was used in the next step without additional purification. Yield: 28.0 g, 0.11 mol, >100percent. |