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[ CAS No. 1244058-73-8 ] {[proInfo.proName]}

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Chemical Structure| 1244058-73-8
Chemical Structure| 1244058-73-8
Structure of 1244058-73-8 * Storage: {[proInfo.prStorage]}
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Product Details of [ 1244058-73-8 ]

CAS No. :1244058-73-8 MDL No. :MFCD16987860
Formula : C6H4ClN3S Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 185.63 Pubchem ID :-
Synonyms :

Safety of [ 1244058-73-8 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 1244058-73-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1244058-73-8 ]

[ 1244058-73-8 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 7321-93-9 ]
  • [ 333-20-0 ]
  • [ 1244058-73-8 ]
YieldReaction ConditionsOperation in experiment
76% With hydrogenchloride; In 1,4-dioxane; water; at 110℃; for 48h; 4,6-Dichloropyridin-3-amine (int-57) (1.5 g, 9.3 mmol) and potassium thiocyanate (2.69 g, 27.8 mmol) were dissolved in dioxane (30 mL) and concentrated aq. HC1 (0.1 mL) was added. The solution was stirred at 1 1() C for 2 days. Then, the solvent was removed under reduced pressure, and the residue was purified by column chromatography on silica gel using a mixture of petroleum ether and EtOAc (1:1) as eluent to give 6-chlorothiazolo[4,5-cjpyridin-2-arnine (int?58) (1.3 g, 76percent yield) as a yellow solid. MS (ESI): mz 185.9 [M+H].
  • 2
  • [ 7321-93-9 ]
  • [ 1244058-73-8 ]
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