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Chemical Structure| 1256961-17-7 Chemical Structure| 1256961-17-7

Structure of 1256961-17-7

Chemical Structure| 1256961-17-7

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Product Details of [ 1256961-17-7 ]

CAS No. :1256961-17-7
Formula : C10H10N2O3
M.W : 206.20
SMILES Code : O=C1N(CC)CC2=C1C=CC([N+]([O-])=O)=C2
MDL No. :MFCD27987268

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Application In Synthesis of [ 1256961-17-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1256961-17-7 ]

[ 1256961-17-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 133446-99-8 ]
  • [ 75-04-7 ]
  • [ 1256961-17-7 ]
YieldReaction ConditionsOperation in experiment
85% In tetrahydrofuran; at 20℃; for 3h; Ui) 2-Ethyl-5-nitro-2,3-dihydro-isoindol-l-one2-Bromomethyl-4-nitro-benzoic acid methyl ester (1.0 g, 3.64 mmol) was stirred in ethylamine (30 ml, 2.0M solution in THF) at room temperature. The reaction was stirred for 3 hrs, after which time the solvent was evaporated in vacuo and the crude residue triturated with diethyl ether. The resulting orange solid was filtered and dried in a vacuum oven (400C) to afford the title compound (634 mg, 85%). HPLC retention time 3.56min. Mass spectrum (ES+) m/z 207 (M+H).
 

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