Home Cart 0 Sign in  

[ CAS No. 128-59-6 ] {[proInfo.proName]}

,{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]}
Chemical Structure| 128-59-6
Chemical Structure| 128-59-6
Structure of 128-59-6 * Storage: {[proInfo.prStorage]}
Cart0 Add to My Favorites Add to My Favorites Bulk Inquiry Inquiry Add To Cart

Quality Control of [ 128-59-6 ]

Related Doc. of [ 128-59-6 ]

Alternatived Products of [ 128-59-6 ]

Product Details of [ 128-59-6 ]

CAS No. :128-59-6 MDL No. :MFCD00034580
Formula : C34H16O4 Boiling Point : -
Linear Structure Formula :- InChI Key :MGYICCKROPVHMA-UHFFFAOYSA-N
M.W : 488.49 Pubchem ID :5354980
Synonyms :

Safety of [ 128-59-6 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P280-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H332-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 128-59-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 128-59-6 ]
  • Downstream synthetic route of [ 128-59-6 ]

[ 128-59-6 ] Synthesis Path-Upstream   1~6

  • 1
  • [ 128-59-6 ]
  • [ 7697-37-2 ]
  • [ 116-71-2 ]
Reference: [1] Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 22, p. 1112
[2] Patent: US2075455, 1934, ,
  • 2
  • [ 128-58-5 ]
  • [ 128-59-6 ]
Reference: [1] Patent: CN103804163, 2016, B, . Location in patent: Paragraph 0028; 0029; 0030; 0031; 0032
  • 3
  • [ 116-71-2 ]
  • [ 128-59-6 ]
Reference: [1] Patent: US2278987, 1940, ,
[2] Promysl.org.Chim., 1936, vol. 2, p. 576[3] Chem. Zentralbl., 1937, vol. 108, # I, p. 2871
[4] Patent: US2278987, 1940, ,
[5] Promysl.org.Chim., 1936, vol. 2, p. 576[6] Chem. Zentralbl., 1937, vol. 108, # I, p. 2871
[7] Patent: US2278987, 1940, ,
[8] Promysl.org.Chim., 1936, vol. 2, p. 576[9] Chem. Zentralbl., 1937, vol. 108, # I, p. 2871
[10] Patent: US2278987, 1940, ,
[11] Promysl.org.Chim., 1936, vol. 2, p. 576[12] Chem. Zentralbl., 1937, vol. 108, # I, p. 2871
[13] Patent: US2278987, 1940, ,
[14] Promysl.org.Chim., 1936, vol. 2, p. 576[15] Chem. Zentralbl., 1937, vol. 108, # I, p. 2871
[16] Patent: US2278987, 1940, ,
[17] Promysl.org.Chim., 1936, vol. 2, p. 576[18] Chem. Zentralbl., 1937, vol. 108, # I, p. 2871
[19] Patent: US2278987, 1940, ,
[20] Promysl.org.Chim., 1936, vol. 2, p. 576[21] Chem. Zentralbl., 1937, vol. 108, # I, p. 2871
[22] Patent: US2278987, 1940, ,
[23] Promysl.org.Chim., 1936, vol. 2, p. 576[24] Chem. Zentralbl., 1937, vol. 108, # I, p. 2871
[25] Patent: US2278987, 1940, ,
[26] Promysl.org.Chim., 1936, vol. 2, p. 576[27] Chem. Zentralbl., 1937, vol. 108, # I, p. 2871
[28] Patent: US2278987, 1940, ,
[29] Promysl.org.Chim., 1936, vol. 2, p. 576[30] Chem. Zentralbl., 1937, vol. 108, # I, p. 2871
[31] Patent: US2278987, 1940, ,
[32] Promysl.org.Chim., 1936, vol. 2, p. 576[33] Chem. Zentralbl., 1937, vol. 108, # I, p. 2871
[34] Patent: US2278987, 1940, ,
[35] Promysl.org.Chim., 1936, vol. 2, p. 576[36] Chem. Zentralbl., 1937, vol. 108, # I, p. 2871
[37] Patent: US2278987, 1940, ,
[38] Promysl.org.Chim., 1936, vol. 2, p. 576[39] Chem. Zentralbl., 1937, vol. 108, # I, p. 2871
[40] Patent: US2278987, 1940, ,
[41] Promysl.org.Chim., 1936, vol. 2, p. 576[42] Chem. Zentralbl., 1937, vol. 108, # I, p. 2871
[43] Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 11, p. 698
[44] Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 11, p. 698
[45] J.Soc.chem.Ind.Japan Spl., vol. 38, p. 640 B[46] Chem. Zentralbl., 1936, vol. 107, # II, p. 469
[47] Dyes and Pigments, 2012, vol. 95, # 2, p. 377 - 383
[48] Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 11, p. 698
[49] Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 11, p. 698
  • 4
  • [ 82-05-3 ]
  • [ 128-59-6 ]
Reference: [1] Patent: US1967617, 1932, ,
  • 5
  • [ 116-90-5 ]
  • [ 128-59-6 ]
Reference: [1] Kogyo Kagaku Zasshi, 1943, vol. 46, p. 1256[2] Chem.Abstr., 1948, p. 6119
  • 6
  • [ 111-83-1 ]
  • [ 128-59-6 ]
  • [ 85652-50-2 ]
YieldReaction ConditionsOperation in experiment
72% With 18-crown-6 ether; potassium carbonate In 1-methyl-pyrrolidin-2-one at 100℃; for 8 h; Taking 1.21g (2.48mmol) 16, 17-dihydroxy Anthracyclinone purple puts in 100 ml flask, add 50mLN-methyl pyrrolidone, heating 10 min to 100 °C the 16, 17-dihydroxy Anthracyclinone purple disperse as much as possible. Then add 1.00g (7.2mmol) no water K2CO3, 0.98g (5.08mmol) 1-polybromide octane, and presence of 18-crown -6. Maintain reaction temperature 100 °C, reaction 8 hours the reaction is stopped.The reaction solution is poured into 100 ml water, fully mixing, filtering, drying to obtain the crude product. Dichloromethane is used for dissolving the crude product, filtering to remove undissolved components. turns on lathe does dichloromethane, to obtain the solid, dried to obtain 1.26g grams of product, yield is 72percent. The silica gel chromatographic column, to CH2Cl2: CH3OH=20 1 as eluant, further elution separation and purification.
Reference: [1] Patent: CN103804163, 2016, B, . Location in patent: Paragraph 0036; 0037; 0038
[2] Frontiers of Chemistry in China, 2010, vol. 5, # 2, p. 200 - 207
[3] Dyes and Pigments, 2012, vol. 95, # 2, p. 377 - 383
Same Skeleton Products
Historical Records