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Chemical Structure| 1284246-87-2 Chemical Structure| 1284246-87-2

Structure of 1284246-87-2

Chemical Structure| 1284246-87-2

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Product Details of [ 1284246-87-2 ]

CAS No. :1284246-87-2
Formula : C11H22N2O3
M.W : 230.30
SMILES Code : O=C(OC(C)(C)C)NCCNC1COCC1

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Application In Synthesis of [ 1284246-87-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1284246-87-2 ]

[ 1284246-87-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 88675-24-5 ]
  • [ 39684-80-5 ]
  • [ 1284246-87-2 ]
YieldReaction ConditionsOperation in experiment
With potassium carbonate; In N,N-dimethyl-formamide; at 50℃; for 16h; A suspension of (+/-)-tetrahydro~3-furanamine (1.1 g, 8.90 mmol, Small Molecules Inc., NJ, USA), 1 ,1-dimethyIethyl (2-bromoethy.)carbamate (1.995 g, 8.90 mmol), and potassium carbonate (3.69 g, 26.7 mmol) in N.N-dimethylformannide (15 mL) was maintained at 50 °C in a sealed pressure vessel for 16 hours. The mixture was cooled, diluted with ethyi acetate, and poured into water. The organic layer was washed twice with 5percent LiCI (aqueous), dried over sodium sulfate, and taken to a residue under reduced pressure to afford 1 ,1-dimethylethyl [2-(tetrahydro-3- furanylamino)ethyl]carbamate (1.33 g, 5.77 mmol, 65percent yield, roughly 50percent purity) as a clear oil used immediately in the subsequent transformation
 

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