Home Cart 0 Sign in  

[ CAS No. 129410-28-2 ] {[proInfo.proName]}

,{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]}
Chemical Structure| 129410-28-2
Chemical Structure| 129410-28-2
Structure of 129410-28-2 * Storage: {[proInfo.prStorage]}
Cart0 Add to My Favorites Add to My Favorites Bulk Inquiry Inquiry Add To Cart

Quality Control of [ 129410-28-2 ]

Related Doc. of [ 129410-28-2 ]

Alternatived Products of [ 129410-28-2 ]

Product Details of [ 129410-28-2 ]

CAS No. :129410-28-2 MDL No. :MFCD00960730
Formula : C18H21N7 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 335.41 Pubchem ID :-
Synonyms :

Safety of [ 129410-28-2 ]

Signal Word: Class:
Precautionary Statements: UN#:
Hazard Statements: Packing Group:

Application In Synthesis of [ 129410-28-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 129410-28-2 ]

[ 129410-28-2 ] Synthesis Path-Downstream   1~16

  • 1
  • [ 95-14-7 ]
  • [ 50-00-0 ]
  • [ 109-73-9 ]
  • [ 129410-28-2 ]
YieldReaction ConditionsOperation in experiment
76% With toluene-4-sulfonic acid In water
In water at 20℃; for 0.5h; Yield given;
  • 2
  • [ 100-42-5 ]
  • [ 129410-28-2 ]
  • 1-butyl-3-phenylpyrrolidine [ No CAS ]
YieldReaction ConditionsOperation in experiment
59% With samarium diiodide In various solvent(s)
  • 3
  • [ 622-97-9 ]
  • [ 129410-28-2 ]
  • 1-butyl-3-(4'-methylphenyl)pyrrolidine [ No CAS ]
YieldReaction ConditionsOperation in experiment
53% With samarium diiodide In various solvent(s)
  • 4
  • [ 405-99-2 ]
  • [ 129410-28-2 ]
  • 1-butyl-3-(4'-fluorophenyl)pyrrolidine [ No CAS ]
YieldReaction ConditionsOperation in experiment
40% With samarium diiodide In various solvent(s)
  • 5
  • [ 129410-28-2 ]
  • [ 754-05-2 ]
  • 1-butyl-3-trimethylsilylpyrrolidine [ No CAS ]
YieldReaction ConditionsOperation in experiment
85% With samarium diiodide In various solvent(s)
  • 6
  • [ 129410-28-2 ]
  • [ 2227-79-4 ]
  • 3-butyl-6-phenyl-3,4-dihydro-2H-1,3,5-thiadiazine [ No CAS ]
YieldReaction ConditionsOperation in experiment
78% With zinc dibromide In dichloromethane at 20℃; for 48h;
  • 7
  • [ 118-72-9 ]
  • [ 129410-28-2 ]
  • 3-butyl-9-methyl-2,3,4,5-tetrahydro-1,3-benzothiazepine [ No CAS ]
YieldReaction ConditionsOperation in experiment
65% Stage #1: 2,6-dimethylbenzene-1-thiol With n-butyllithium; N,N,N,N,-tetramethylethylenediamine In hexane; cyclohexane at 20℃; for 24h; Stage #2: N,N-bis(1H-1,2,3-benzotriazol-1-ylmethyl)butan-1-amine With N,N,N,N,-tetramethylethylenediamine; zinc dibromide In tetrahydrofuran; hexane; cyclohexane at 20℃; for 24h; Further stages.;
  • 8
  • [ 93-98-1 ]
  • [ 129410-28-2 ]
  • 2-phenyl-4-butyl-2,3,4,5-tetrahydro-1H-2,4-benzodiazepin-1-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
47% Stage #1: N-phenyl benzoyl amide With n-butyllithium In tetrahydrofuran at -10 - 0℃; for 0.5h; Stage #2: N,N-bis(1H-1,2,3-benzotriazol-1-ylmethyl)butan-1-amine With zinc dibromide In tetrahydrofuran at -10 - 20℃; for 24h; Further stages.;
  • 9
  • [ 88070-48-8 ]
  • [ 129410-28-2 ]
  • 2-methyl-4-butyl-2,3,4,5-tetrahydro-1H-2,4-benzodiazepin-1-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
64% Stage #1: N-methylbenzamide With n-butyllithium In tetrahydrofuran at -10 - 0℃; for 0.5h; Stage #2: N,N-bis(1H-1,2,3-benzotriazol-1-ylmethyl)butan-1-amine With zinc dibromide In tetrahydrofuran at -10 - 20℃; for 24h; Further stages.;
  • 10
  • [ 2866-82-2 ]
  • [ 129410-28-2 ]
  • 2-(4-chlorophenyl)-4-butyl-2,3,4,5-tetrahydro-1H-2,4-benzodiazepin-1-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
57% Stage #1: N-(4-chlorophenyl)benzamide With n-butyllithium In tetrahydrofuran at -10 - 0℃; for 0.5h; Stage #2: N,N-bis(1H-1,2,3-benzotriazol-1-ylmethyl)butan-1-amine With zinc dibromide In tetrahydrofuran at -10 - 20℃; for 24h; Further stages.;
  • 11
  • [ 5894-65-5 ]
  • [ 129410-28-2 ]
  • 2-(tert-butyl)-4-butyl-2,3,4,5-tetrahydro-1H-2,4-benzodiazepin-1-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
82% Stage #1: N-t-butylbenzamide With n-butyllithium In tetrahydrofuran at -10 - 0℃; for 0.5h; Stage #2: N,N-bis(1H-1,2,3-benzotriazol-1-ylmethyl)butan-1-amine With zinc dibromide In tetrahydrofuran at -10 - 20℃; for 24h; Further stages.;
  • 12
  • [ 129410-28-2 ]
  • [ 108-98-5 ]
  • 3-butyl-3,4-dihydro-2H-1,3-benzothiazine [ No CAS ]
YieldReaction ConditionsOperation in experiment
44% Stage #1: thiophenol With n-butyllithium; N,N,N,N,-tetramethylethylenediamine In hexane; cyclohexane at 20℃; for 19h; Stage #2: N,N-bis(1H-1,2,3-benzotriazol-1-ylmethyl)butan-1-amine With N,N,N,N,-tetramethylethylenediamine; zinc dibromide In tetrahydrofuran; hexane; cyclohexane at 20℃; Further stages.;
  • 13
  • [ 129410-28-2 ]
  • [ 106-45-6 ]
  • 3-butyl-6-methyl-3,4-dihydro-2H-1,3-benzothiazine [ No CAS ]
YieldReaction ConditionsOperation in experiment
58% Stage #1: para-thiocresol With n-butyllithium; N,N,N,N,-tetramethylethylenediamine In hexane; cyclohexane at 20℃; for 19h; Stage #2: N,N-bis(1H-1,2,3-benzotriazol-1-ylmethyl)butan-1-amine With N,N,N,N,-tetramethylethylenediamine; zinc dibromide In tetrahydrofuran; hexane; cyclohexane at 20℃; Further stages.;
  • 14
  • [ 129410-28-2 ]
  • [ 137-06-4 ]
  • 3-butyl-8-methyl-3,4-dihydro-2H-1,3-benzothiazine [ No CAS ]
  • 3-butyl-2,3,4,5-tetrahydro-1,3-benzothiazepine [ No CAS ]
YieldReaction ConditionsOperation in experiment
25% Stage #1: 2-thiocresol With n-butyllithium; N,N,N,N,-tetramethylethylenediamine In hexane; cyclohexane at 20℃; for 19h; Stage #2: N,N-bis(1H-1,2,3-benzotriazol-1-ylmethyl)butan-1-amine With N,N,N,N,-tetramethylethylenediamine; zinc dibromide In tetrahydrofuran; hexane; cyclohexane at 20℃;
1: 20% 2: 25% Stage #1: 2-thiocresol With n-butyllithium; N,N,N,N,-tetramethylethylenediamine In hexane; cyclohexane at 20℃; for 19h; Stage #2: N,N-bis(1H-1,2,3-benzotriazol-1-ylmethyl)butan-1-amine With N,N,N,N,-tetramethylethylenediamine; zinc dibromide In tetrahydrofuran; hexane; cyclohexane at 20℃;
  • 15
  • [ 129410-28-2 ]
  • [ 137-06-4 ]
  • 3-butyl-2,3,4,5-tetrahydro-1,3-benzothiazepine [ No CAS ]
YieldReaction ConditionsOperation in experiment
45% Stage #1: 2-thiocresol With n-butyllithium; N,N,N,N,-tetramethylethylenediamine In hexane; cyclohexane at 20℃; for 24h; Stage #2: N,N-bis(1H-1,2,3-benzotriazol-1-ylmethyl)butan-1-amine With N,N,N,N,-tetramethylethylenediamine; zinc dibromide In tetrahydrofuran; hexane; cyclohexane at 20℃; for 24h; Further stages.;
  • 16
  • [ 129410-28-2 ]
  • [ 108-95-2 ]
  • 3-butyl-3,4-dihydro-2H-benzo[e]-1,3-oxazine [ No CAS ]
YieldReaction ConditionsOperation in experiment
70% Stage #1: phenol With n-butyllithium; N,N,N,N,-tetramethylethylenediamine In hexane; cyclohexane at 20℃; for 8h; Stage #2: N,N-bis(1H-1,2,3-benzotriazol-1-ylmethyl)butan-1-amine With N,N,N,N,-tetramethylethylenediamine; zinc dibromide In tetrahydrofuran; hexane; cyclohexane at 20℃; Further stages.;
Same Skeleton Products
Historical Records