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[ CAS No. 13058-73-6 ]

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Chemical Structure| 13058-73-6
Chemical Structure| 13058-73-6
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Product Details of [ 13058-73-6 ]

CAS No. :13058-73-6 MDL No. :MFCD09264588
Formula : C9H6N2O2 Boiling Point : 353.3°C at 760 mmHg
Linear Structure Formula :- InChI Key :-
M.W :174.16 g/mol Pubchem ID :-
Synonyms :

Safety of [ 13058-73-6 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 13058-73-6 ]

  • Upstream synthesis route of [ 13058-73-6 ]
  • Downstream synthetic route of [ 13058-73-6 ]

[ 13058-73-6 ] Synthesis Path-Upstream   1~2

  • 1
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  • [ 23707-37-1 ]
YieldReaction ConditionsOperation in experiment
90% With palladium 10% on activated carbon; hydrogen In methanol at 20℃; for 24.5 h; Synthesis of isoquinolin-7-amine (31-4)
To a suspend solution of Pd/C (10percent, 100 mg) in methanol (20 mL) was added 31-3 (200 mg, 1.15 mmol) in methanol (40 mL).
After having been degassed and recharged with hydrogen, the mixture was then stirred at room temperature for 24.5 h. TLC showed that the reaction was complete.
The Pd/C was removed by filtration and the solvent was evaporated.
The residual was used without further purification (150 mg, yield 90percent).
Reference: [1] Patent: US9138427, 2015, B2, . Location in patent: Page/Page column 307
[2] Journal of the Chemical Society, 1951, p. 2851
[3] Patent: US5807886, 1998, A,
[4] Journal of the American Chemical Society, 2011, vol. 133, # 20, p. 8014 - 8027
[5] Synlett, 2013, vol. 24, # 3, p. 301 - 304
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  • [ 58794-09-5 ]
Reference: [1] Journal of the American Chemical Society, 2011, vol. 133, # 20, p. 8014 - 8027
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