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CAS No. : | 1309208-83-0 | MDL No. : | MFCD28246274 |
Formula : | C7H10F3NO3 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 213.15 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Class: | ||
Precautionary Statements: | UN#: | ||
Hazard Statements: | Packing Group: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
100% | In dichloromethane; at 20℃; for 4h; | Step 4: l-Azetidin-3- -ethanoneTrifluoroacetic acid (8 mL) was added to a suspension of 3-acetyl-azetidine-l- carboxylic acid terf-butyl ester (800 mg, 4.0 mmol) in dichloromethane (20 mL). The reaction mixture was stirred at room temperature for 4 hours and concentrated to dryness to afford the title product as a colorless gum (800 mg, 100percent).*H NMR (400 MHz, DMSO-c/6) delta (ppm) : 4.02-4.06 (m, 4H), 3.75-3.80 (m, 1H), 2.13 (s, 3H). |