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[ CAS No. 1312903-94-8 ] {[proInfo.proName]}

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Chemical Structure| 1312903-94-8
Chemical Structure| 1312903-94-8
Structure of 1312903-94-8 * Storage: {[proInfo.prStorage]}
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Product Details of [ 1312903-94-8 ]

CAS No. :1312903-94-8 MDL No. :MFCD23135680
Formula : C10H13NO3 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 195.22 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 1312903-94-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1312903-94-8 ]

[ 1312903-94-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 77199-09-8 ]
  • [ 1312903-94-8 ]
YieldReaction ConditionsOperation in experiment
20% With sodium; In ethanol; for 3h;Reflux; (b) Preparation of ethyl 5-ethoxypyridine-2-carboxylate 3 :To a solution of <strong>[77199-09-8]ethyl 5-bromopyridine-2-carboxylate</strong> 2 (1.5 g, 6.5 mmol) in 20 mL of EtOH was added a solution of sodium (0.18 g, 7.8 mmol) in 20 mL of EtOH. The mixture was stirred at reflux for 3 h. After removal of all solvent, the residue was purified by column (2: 1 of hexane/ethyl acetate) to give ethyl 5-ethoxypyridine-2-carboxylate 3 as an oil. Yield: 0.26 g, 20%. .HNMR (CDCI3) delta (ppm): 8.38 (d, 1 H), 8.10 (d, 1 H), 8.23 (d, 1 H), 7.22 (dd, 1 H), 4.45 (m, 2 H), 4.25 (m, 1 H), 1.40 (m, 6 H).
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