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Chemical Structure| 13266-02-9 Chemical Structure| 13266-02-9

Structure of 13266-02-9

Chemical Structure| 13266-02-9

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Product Details of [ 13266-02-9 ]

CAS No. :13266-02-9
Formula : C31H42BrP
M.W : 525.54
SMILES Code : CCCCCCCCCCCCC[P+](C1=CC=CC=C1)(C2=CC=CC=C2)C3=CC=CC=C3.[Br-]

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Application In Synthesis of [ 13266-02-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 13266-02-9 ]

[ 13266-02-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 116754-58-6 ]
  • [ 603-35-0 ]
  • [ 13266-02-9 ]
YieldReaction ConditionsOperation in experiment
95% In acetonitrile; for 48h;Reflux; Inert atmosphere; <strong>[116754-58-6]13-bromo-1-tridecanol</strong> (13.9 g, 50 mmol) was placed in a 250 mL three-neck round bottom flask,Triphenylphosphine (13.1 g, 55 mmol) and anhydrous acetonitrile (60 mL), the reaction mixture was stirred at reflux for 48 h under the protection of nitrogen.After the reaction was completed, the solvent was distilled off under reduced pressure, and the obtained residue was repeatedly stirred with anhydrous ether,Until a large amount of white precipitate appeared. After filtering under reduced pressure, vacuum drying for several hours,Tridecyl triphenylphosphine bromide (25.7 g, 95%) was obtained.
 

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