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Chemical Structure| 13438-29-4 Chemical Structure| 13438-29-4

Structure of 13438-29-4

Chemical Structure| 13438-29-4

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Product Details of [ 13438-29-4 ]

CAS No. :13438-29-4
Formula : C9H6Cl2O2
M.W : 217.05
SMILES Code : O=C(Cl)C1=CC(C)=CC(C(Cl)=O)=C1

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Application In Synthesis of [ 13438-29-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 13438-29-4 ]

[ 13438-29-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 499-49-0 ]
  • [ 13438-29-4 ]
YieldReaction ConditionsOperation in experiment
With thionyl chloride; at 50℃; for 18h; Step 1. N,N'-dimethoxy-N,N',5-trimethylisophthalamide (4a). To a 200 mL round bottomed flask with a stirring bar, reflux condenser and a drying tube was added <strong>[499-49-0]5-methylisophthalic acid</strong> (10.00 g, 55.51 mmol) and thionyl chloride (50.0 mL, 685.47 mmol). This mixture was heated at 50° C. 18h. The excess thionyl chloride was removed in vacuo to give solid crude diacid chloride.
 

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