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[ CAS No. 13440-22-7 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 13440-22-7
Chemical Structure| 13440-22-7
Structure of 13440-22-7 * Storage: {[proInfo.prStorage]}
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Product Details of [ 13440-22-7 ]

CAS No. :13440-22-7 MDL No. :MFCD12974038
Formula : C8H11NO2S Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 185.24 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 13440-22-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 13440-22-7 ]

[ 13440-22-7 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 13440-22-7 ]
  • [ 15448-99-4 ]
  • 2
  • [ 13440-22-7 ]
  • [ 15448-99-4 ]
  • [ 81-07-2 ]
  • 3
  • [ 67-56-1 ]
  • [ 88-19-7 ]
  • [ 13440-22-7 ]
YieldReaction ConditionsOperation in experiment
96% With [(Cp*IrCl)2(4,4′,6,6′-tetrahydroxy-2,2′-bipyrimidine)][Cl]2; potassium hydroxide In water at 130℃; for 12h; 4 N,2-dimethylbenzenesulfonamide Combine o-methylbenzenesulfonamide (85.6 mg, 0.5 mmol), iridium catalyst (5.1 mg, 0.005 mmol, 1 mol%), potassium hydroxide (28 mg, 0.5 mmol, 1 equiv), then methanol (0.3 mL) and water (0.9 mL) were added to the reaction vessel in sequence. After the reaction mixture was reacted at 130 ° C for 12 hours in a reaction vessel, it was cooled to room temperature. The solvent was removed by rotary evaporation, and then the purified target compound was obtained by column chromatography (developing solvent: petroleum ether / ethyl acetate), yield: 96%.
92% With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; sodium hydroxide at 150℃; for 12h; Inert atmosphere; Schlenk technique; Green chemistry;
91% With [(Cp*IrCl)2(4,4′,6,6′-tetrahydroxy-2,2′-bipyrimidine)][Cl]2; potassium hydroxide In water at 130℃; for 12h; Schlenk technique;
90% With [Cp*Ir(2-(1H-benzo[d]imidazol-2-yl)-1H-benzo[d]imidazole)Cl][Cl]; caesium carbonate at 120℃; for 12h; Schlenk technique;

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