Alternatived Products of [ 1344121-06-7 ]
Product Details of [ 1344121-06-7 ]
CAS No. : | 1344121-06-7 |
MDL No. : | N/A |
Formula : |
C24H33B2NO4
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
421.15
|
Pubchem ID : | - |
Synonyms : |
|
Safety of [ 1344121-06-7 ]
Application In Synthesis of [ 1344121-06-7 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 1344121-06-7 ]
- 1
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[ 16292-17-4 ]
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[ 73183-34-3 ]
-
bis(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)amine
[ No CAS ]
Yield | Reaction Conditions | Operation in experiment |
80% |
With tetrakis(triphenylphosphine) palladium(0); In 1,4-dioxane; for 12h;Reflux; Inert atmosphere; |
General procedure: Reactant 1 (2 g, 4.7 mmol), 3bromo1propanol (1.33 g,9.5 mmol), and Pd(PPh34 (2.4 g, 0.02 mmol) were dissolvedin distilled THF (50 mL). The potassium carbonatesolution (2 N, 20 mL) was added to the mixtureand the reaction mixture was refluxed for 12 hours undernitrogen. The reaction was then cooled to room temperatureand diluted with an equal volume of water. Theresulting mixture was extracted with methylene chloride(three times), washed with sodium bicarbonate solution,and dried over magnesium sulfate (MgSO4. After the solventwas removed under vacuum, the crude material waspurified by column chromatography on silica gel (methylenechloride: hexane=1:7 as eluent) to give the title compound2 (yield: 65%). |