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Chemical Structure| 134606-34-1 Chemical Structure| 134606-34-1

Structure of 134606-34-1

Chemical Structure| 134606-34-1

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Product Details of [ 134606-34-1 ]

CAS No. :134606-34-1
Formula : C25H46O14P2
M.W : 632.57
SMILES Code : O=C(C(C)(C)C)OCOP(OCOC(C(C)(C)C)=O)(CP(OCOC(C(C)(C)C)=O)(OCOC(C(C)(C)C)=O)=O)=O
MDL No. :MFCD34663338

Safety of [ 134606-34-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319
Precautionary Statements:P501-P270-P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330

Application In Synthesis of [ 134606-34-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 134606-34-1 ]

[ 134606-34-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 18997-19-8 ]
  • [ 16001-93-7 ]
  • [ 134606-34-1 ]
YieldReaction ConditionsOperation in experiment
45% With sodium iodide; In acetonitrile;Reflux; Tetramethyl methylenebisphosphonate (120 g, 0.51 mol), Nal (308 g, 2 mol), chloromethyl pivalate (387 g, 2.5 mol) and acetonitrile (400 ml) were mixed and refluxed overnight. TLC (thin-layer chromatography) in EtOAc with 5 % methanol confirmed the formation of product. The reaction mixture was diluted with ether (1000 ml) and washed with water (2 x 1000 ml), dried with Na2S03and evaporated. The solid residue was washed with cold hexane and dried in vacuum to give 148 g (45 %) of X as a pale yellow solid. NM (500 MHz, CDCI3): d 5.73-5.63 (m, 8H), 2.65 (t, 2H), 1.22 (s, 36H);31P NM (500 MHz, CDCI3): d 18.61.
 

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