Home Cart Sign in  
Chemical Structure| 1351394-96-1 Chemical Structure| 1351394-96-1

Structure of 1351394-96-1

Chemical Structure| 1351394-96-1

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 1351394-96-1 ]

CAS No. :1351394-96-1
Formula : C31H25P
M.W : 428.50
SMILES Code : CC1=CC=CC(C2=CC=CC=C2)=C1C3=C(P(C4=CC=CC=C4)C5=CC=CC=C5)C=CC=C3

Safety of [ 1351394-96-1 ]

Application In Synthesis of [ 1351394-96-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1351394-96-1 ]

[ 1351394-96-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 108-86-1 ]
  • [ 402822-72-4 ]
  • [ 1351394-96-1 ]
YieldReaction ConditionsOperation in experiment
83% With chloro(1,5-cyclooctadiene)rhodium(I) dimer; lithium tert-butoxide; In 1,4-dioxane; at 138℃; for 36h;Schlenk technique; Inert atmosphere; 25 mL of Schlenk tube, 70.5 mg (0.2 mmol) of <strong>[402822-72-4]2-diphenylphosphino-2'-methylbiphenyl</strong> was added,(1,5-cyclooctadiene) chlorineRhodium (I) dimer 2.5 mg (2.5% of the molar number of raw materials)Lithium tert-butanol (48 mg, 0.6 mmol) was added, and argon was replaced three times, and 1 mL of 1,4-dioxane and 47.1 mg (0.3 mmol) of bromobenzene were added under argon. 138 C for 36 hours and cooled to room The solvent was distilled off under reduced pressure, separated by 200-300 mesh silica gel column, petroleum ether: ethyl acetate = 100: 1, vacuum After drying the product was 69.9 mg of a white solid in 83% yield.
 

Historical Records