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Chemical Structure| 1374144-48-5 Chemical Structure| 1374144-48-5

Structure of 1374144-48-5

Chemical Structure| 1374144-48-5

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Product Details of [ 1374144-48-5 ]

CAS No. :1374144-48-5
Formula : C15H22BrN3O2
M.W : 356.26
SMILES Code : O=C(N1CCN(CC2=NC=CC(Br)=C2)CC1)OC(C)(C)C
MDL No. :MFCD31725119

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Application In Synthesis of [ 1374144-48-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1374144-48-5 ]

[ 1374144-48-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 131747-63-2 ]
  • [ 57260-71-6 ]
  • [ 1374144-48-5 ]
YieldReaction ConditionsOperation in experiment
68% With sodium tris(acetoxy)borohydride; acetic acid; In dichloromethane; at 20℃; Sodium triacetoxyborohydride (0.85 g, 4.01 mmol) was added to a solution of <strong>[131747-63-2]4-bromopicolinaldehyde</strong> (0.25 g, 1.34 mmol), tert-butyl piperazine-1-carboxylate (0.28 g,1.48 mmol) and acetic acid (0.02 mL, 0.4 mmol) in dichloromethane (5 mL) and the resulting mixture was stirred overnight at room temperature. The solvent was then evaporated and the residue was triturated with diethyl ether, filtered and the solvent evaporated in vacuo. The residue was purified by flash chromatography to yield the titlecompound (363 mg, 68percent) as a solid. LRMS (m/z): 356/358 (M+1).1H-NMR (300 MHz, CDCI3): 1.46 (s, 9H), 2.46 (t, 4H), 3.46 (t, 4H), 3.64 (s, 2H), 7.62 (d, 1H), 8.37 (d, 1H).
 

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