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Chemical Structure| 1384579-30-9 Chemical Structure| 1384579-30-9

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Chemical Structure| 1384579-30-9

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Product Details of [ 1384579-30-9 ]

CAS No. :1384579-30-9
Formula : C15H20INO4S
M.W : 437.29
SMILES Code : O=C(C1=C(I)SC2=C1CCN(C(OC(C)(C)C)=O)C2)OCC

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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1384579-30-9 ]

[ 1384579-30-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 193537-14-3 ]
  • [ 1384579-30-9 ]
YieldReaction ConditionsOperation in experiment
52% With copper(l) iodide; tert.-butylnitrite; In acetonitrile; at 0℃; for 0.166667h; General procedure: Condition B: To a solution of tert-butyl nitrite (0.27 mL, 2.30 mmol) and CuI (0.29 g, 1.53 mmol) in MeCN (5 mL) was added compound 2d (0.5 g, 1.53 mmol). The reaction mixture was stirred for 10 min and then solvent was removed under low vacuum. The residue was treated with water (15 mL) and extracted with ethyl acetate (3 x 30 mL). The organic layers were collected, combined, dried over anhydrous Na2SO4, filtered and evaporated under low vacuum. The crude product was purified by column chromatography using 9:1 hexane/ethyl acetate to give of compound 3d; yield: 52% (0.34g); light yellow liquid; 1H NMR (400 MHz, CDCl3) delta: 1.23 (t, J = 4.2 Hz, 3H), 1.52 (s, 9H), 2.98 (bs, 2H), 3.61 (bs, 2H), 4.31 (q, J = 6.8 Hz, 2H), 4.60 (bs, 2H); 13C NMR (100 MHz, CDCl3) delta: 14.3 (2C), 28.4 (3C), 40.6, 42.3 (2C), 60.3, 79.9, 131.2, 140.0, 144.0, 158.8, 162.8; IR (KBr) vmax (cm-1): 2867, 1713, 1620, 1564, 1105, 797; MS (ESI) m/z: 438.2 [M + H];
 

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