Home Cart Sign in  
Chemical Structure| 1400702-00-2 Chemical Structure| 1400702-00-2

Structure of 1400702-00-2

Chemical Structure| 1400702-00-2

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 1400702-00-2 ]

CAS No. :1400702-00-2
Formula : C9H8BrF
M.W : 215.06
SMILES Code : FC1=CC(Br)=CC2=C1CCC2

Safety of [ 1400702-00-2 ]

Application In Synthesis of [ 1400702-00-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1400702-00-2 ]

[ 1400702-00-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 881189-74-8 ]
  • [ 1400702-00-2 ]
YieldReaction ConditionsOperation in experiment
With triethylsilane; trifluoroacetic acid; at 20℃; To a solution of 6-bromo-4-fluoroindan-l-one (57 mg, 0.26 mmol) in trifluoroacetic acid (1.1 mL) was added triethylsilane (103 ih, 0.65 mmol), and the mixture was stirred at room temperature overnight. The reaction solution was poured into ice water, and the mixture was extracted with ethyl acetate three times. The organic layer was combined, washed with saturated aqueous sodium hydrogen carbonate solution, and the organic layer was filtered through Phase-separator (Varian Inc.), and then concentrated under reduced pressure. The resulting residue was purified by silica gel column chromatography (hexane:ethyl acetate = 100:0) to give a crude 6-bromo-4-fluoroindane (61 mg) as a yellow oil. The resultant was used in the next step without further purification.
 

Historical Records