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CAS No. : | 14108-60-2 | MDL No. : | MFCD00070216 |
Formula : | C13H13NO2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | JPZXHKDZASGCLU-UHFFFAOYSA-N |
M.W : | 215.25 | Pubchem ID : | 250399 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 4 steps 1: 76 percent / trifluoroacetic acid / a) 0 deg C, 2 h, b) RT, overnight 3: 95 percent / 2 N NaOH / ethanol / 37 °C 4: 90 percent |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With 4-methyl-morpholine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; In N,N-dimethyl-formamide; for 1h; | Then add the amino acids and other reagents required to add the side chain according to the peptide solid phase synthesis method. The molar ratio of amino acid feed is: Compound 4: amino acid: HBTU (benzotriazole-N, N, N ', N'-Tetramethyl Isourea hexafluorophosphate): NMM (N-methylmorpholine) = 1: 3: 2.85: 6. Connect 1-naphthylalanine in sequence according to the above method,4-aminomethylcyclohexanoic acid, phenylalanine,Add 3 equivalents of amino acid, add appropriate amount of DMF,Reaction for 1h. Transfer the synthetic product into a cutting tube,Add E solution, shake the cutting reaction for 1h; collect the cutting solution into a centrifuge tube, add 6 times the volume of ice ether,Precipitate on a low speed centrifuge; wash the precipitated crude product three times with ether to obtain the crude product of precursor compound 5.Purification by semi-preparative chromatography gave compound 5PSMA-Ala (Nap) -Cyh-Phe. |
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