Alternatived Products of [ 1416146-93-4 ]
Product Details of [ 1416146-93-4 ]
CAS No. : | 1416146-93-4 |
MDL No. : | N/A |
Formula : |
C9H12ClN3O2
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Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
229.66
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Pubchem ID : | - |
Synonyms : |
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Safety of [ 1416146-93-4 ]
Signal Word: | |
Class: | |
Precautionary Statements: | |
UN#: | |
Hazard Statements: | |
Packing Group: | |
Application In Synthesis of [ 1416146-93-4 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 1416146-93-4 ]
- 1
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[ 1416146-93-4 ]
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[ 1314978-36-3 ]
Yield | Reaction Conditions | Operation in experiment |
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With trifluoroacetic acid In dichloromethane at 20℃; for 0.5h; |
15.B Step B.5-chloropyridazin-3-amine
A mixture of tert-butyl N-(5-chloropyridazin-3-yl)carbamate (1.70 g, 7.40 mmol) and trifluoroacetic acid (15.4 g, 135 mmol, 10.0 mL) in dichloromethane (20 mL) was stirred for 0.5 hour at 20 °C. The reaction mixture was then concentrated under reduced pressure to provide the title compound: LCMS m/z 259.0 [M+H]+. |
|
With trifluoroacetic acid In dichloromethane at 20℃; for 0.5h; |
15.B Step B.5-chloropyridazin-3-amine
A mixture of tert-butyl N-(5-chloropyridazin-3-yl)carbamate (1.70 g, 7.40 mmol) and trifluoroacetic acid (15.4 g, 135 mmol, 10.0 mL) in dichloromethane (20 mL) was stirred for 0.5 hour at 20 °C. The reaction mixture was then concentrated under reduced pressure to provide the title compound: LCMS m/z 259.0 [M+H]+. |