Alternatived Products of [ 1423121-04-3 ]
Product Details of [ 1423121-04-3 ]
CAS No. : | 1423121-04-3 |
MDL No. : | MFCD27991816 |
Formula : |
C11H8FN3S
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
233.27
|
Pubchem ID : | - |
Synonyms : |
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Safety of [ 1423121-04-3 ]
Signal Word: | |
Class: | |
Precautionary Statements: | |
UN#: | |
Hazard Statements: | |
Packing Group: | |
Application In Synthesis of [ 1423121-04-3 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 1423121-04-3 ]
- 1
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[ 34179-62-9 ]
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[ 824-80-6 ]
-
[ 1423121-04-3 ]
Yield | Reaction Conditions | Operation in experiment |
78% |
With copper diacetate; palladium diacetate; In 1,4-dioxane; diethylene glycol dimethyl ether; at 120℃; for 24h; |
General procedure: A reaction vessel was charged with thiazolo[3,2-b]-1,2,4-triazoles 1 (0.5 mmol), sodium arylsulfinates 2 (1 mmol),Pd(OAc)2 (5 mol%), Cu(OAc)2 (2 equiv), and dioxane-diglyme (1:2; 1 mL). The mixture was stirred at 120 C andmonitored by TLC. After the completion of the reaction, themixture was poured into H2O (10 mL), and extracted withEtOAc (3 × 10 mL). The combined extract was dried withanhyd MgSO4. The solvent was removed and the crudeproduct was separated by column chromatography (elutedwith petroleum ether-EtOAc) to give the desired products 3and 4. |