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Chemical Structure| 1439394-79-2 Chemical Structure| 1439394-79-2

Structure of 1439394-79-2

Chemical Structure| 1439394-79-2

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Product Details of [ 1439394-79-2 ]

CAS No. :1439394-79-2
Formula : C32H37N7O4S
M.W : 615.75
SMILES Code : O=C(NCC1=CC=CC(CC(NC2=NN=C(CCCCC3=NN=C(NC(CC4=CC=CC=C4)=O)S3)C=C2)=O)=C1)OC(C)(C)C
MDL No. :N/A

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Application In Synthesis of [ 1439394-79-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1439394-79-2 ]

[ 1439394-79-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 71420-95-6 ]
  • [ 1439394-45-2 ]
  • [ 1439394-79-2 ]
YieldReaction ConditionsOperation in experiment
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 0 - 20℃; A flask was charged with 348 (100 mg, 0.27 mmol), Boc-3-aminomethyl- phenylacetic acid (86 mg, 0.325 mmol) in DMF (2 ml) at 0 C was added HOBT (88 mg, 0.65 mmol) followed by EDCI (156 mg, 0.812 mmol). The resulting mixture was stirred at 0 C for 5 minutes then warmed up to room temperature overnight before it was quenched by addition of water (-10 mL) at 0 C. The white precipitate was collected by suction filtration, rinsed with more water. The crude material was purified by silica gel chromatography eluting with 0-6% MeOH in CH2CI2 to afford 367.
 

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