Purity | Size | Price | VIP Price | USA Stock *0-1 Day | Global Stock *5-7 Days | Quantity | ||||||
{[ item.p_purity ]} | {[ item.pr_size ]} | Inquiry |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,item.pr_rate,1,item.pr_is_large_size_no_price) ]} |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} | Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,1,item.mem_rate,item.pr_is_large_size_no_price) ]} | {[ item.pr_usastock ]} | in stock Inquiry - | {[ item.pr_chinastock ]} | {[ item.pr_remark ]} in stock Inquiry - | Login | Inquiry |
Please Login or Create an Account to: See VIP prices and availability
CAS No. : | 144-80-9 | MDL No. : | MFCD00066501 |
Formula : | C8H10N2O3S | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | SKIVFJLNDNKQPD-UHFFFAOYSA-N |
M.W : | 214.24 | Pubchem ID : | 5320 |
Synonyms : |
Sulphacetamide;Acetosulfamine;Sebizon;Region;NSC63871
|
Chemical Name : | N-((4-Aminophenyl)sulfonyl)acetamide |
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
39.49% | With acetic acid; at 120℃; | General procedure: The compounds were prepared through condensation reaction between 0.001 mol tetrafluorophthalic anhydride and 0.001 mol sulfonamides in 5 mL acetic acid under reflux at 120 C for 3-4 h. Then 20 mL distilled water was added into the reaction media. The compounds were filtered and recrystallized in ethanol. |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
55% | With 3-Methylpyridine; methanesulfonyl chloride; In acetonitrile; at 0 - 20℃; for 1h; | Example 21. Synthesis of N-(4-(N-acetylsulfamoyl)phenyl)-l-methyl-3 -phenyl- 1H- pyrazole-5-carboxamide, 1-97 1-97 [00369] Methanesulfonyl chloride (0.05 ml, 0.65 mmol) was added to a stirred mixture of N- [(4-aminophenyl)sulfonyl]acetamide (100 mg, 0.47 mmol), l-methyl-3 -phenyl- lH-pyrazole-5- carboxylic acid (94mg, 0.47 mmol) and 3-picoline (0.14ml, 1.4 mmol) in MeCN (dry, 5ml) at 0C. After addition the reaction mixture was allowed to reach rt and stirred for lh. The reaction crude was partitioned between DCM (75ml) and water (50ml). The aqueous layer was further extracted with DCM (2 x 50ml) and the combined layers were evaporated to afford a material which was purified by prep HPLC (MeCN /Water, 0.1% formic acid) to obtain 102mg (55%) of N-[4-(acetamidosulfonyl)phenyl] -l-methyl-3 -phenyl- lH-pyrazole-5-carboxamide 1-97 as a colourless solid. 1H NMR (500 MHz, DMSO-d6) delta 12.01 (s, 1H), 10.68 (s, 1H), 7.98 (d, J = 8.9 Hz, 2H), 7.92 (d, J = 8.8 Hz, 2H), 7.82 (d, J = 7.3 Hz, 2H), 7.52 (s, 1H), 7.46 (t, J = 7.7 Hz, 2H), 7.35 (t, 1H), 4.15 (s, 3H), 1.92 (s, 3H). |
[ 127-56-0 ]
Sodium acetyl((4-aminophenyl)sulfonyl)amide
Similarity: 0.99
[ 6209-17-2 ]
Sodium acetyl((4-aminophenyl)sulfonyl)amide hydrate
Similarity: 0.99
[ 459434-40-3 ]
3-Amino-N-methylbenzenesulfonamide
Similarity: 0.84
[ 608523-94-0 ]
N-tert-Butyl 3-Aminophenylsulfonamide
Similarity: 0.83
[ 127-71-9 ]
N-((4-Aminophenyl)sulfonyl)benzamide
Similarity: 0.83
[ 127-56-0 ]
Sodium acetyl((4-aminophenyl)sulfonyl)amide
Similarity: 0.99
[ 6209-17-2 ]
Sodium acetyl((4-aminophenyl)sulfonyl)amide hydrate
Similarity: 0.99
[ 127-71-9 ]
N-((4-Aminophenyl)sulfonyl)benzamide
Similarity: 0.83
[ 414864-00-9 ]
N-Hydroxy-3-(3-(N-phenylsulfamoyl)phenyl)acrylamide
Similarity: 0.75
[ 127-56-0 ]
Sodium acetyl((4-aminophenyl)sulfonyl)amide
Similarity: 0.99
[ 6209-17-2 ]
Sodium acetyl((4-aminophenyl)sulfonyl)amide hydrate
Similarity: 0.99
[ 459434-40-3 ]
3-Amino-N-methylbenzenesulfonamide
Similarity: 0.84
[ 608523-94-0 ]
N-tert-Butyl 3-Aminophenylsulfonamide
Similarity: 0.83
[ 127-71-9 ]
N-((4-Aminophenyl)sulfonyl)benzamide
Similarity: 0.83
[ 127-56-0 ]
Sodium acetyl((4-aminophenyl)sulfonyl)amide
Similarity: 0.99
[ 6209-17-2 ]
Sodium acetyl((4-aminophenyl)sulfonyl)amide hydrate
Similarity: 0.99
[ 459434-40-3 ]
3-Amino-N-methylbenzenesulfonamide
Similarity: 0.84
[ 608523-94-0 ]
N-tert-Butyl 3-Aminophenylsulfonamide
Similarity: 0.83
[ 127-71-9 ]
N-((4-Aminophenyl)sulfonyl)benzamide
Similarity: 0.83