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Chemical Structure| 1440066-11-4 Chemical Structure| 1440066-11-4

Structure of 1440066-11-4

Chemical Structure| 1440066-11-4

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Product Details of [ 1440066-11-4 ]

CAS No. :1440066-11-4
Formula : C31H39B2NO5
M.W : 527.27
SMILES Code : CC(C)(C(C)(C)O1)OB1C(C=C2)=CC=C2N(C3=CC=C(B4OC(C)(C(C)(C)O4)C)C=C3)C(C=C5)=CC=C5OC

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Application In Synthesis of [ 1440066-11-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1440066-11-4 ]

[ 1440066-11-4 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 61676-62-8 ]
  • [ 100308-69-8 ]
  • [ 1440066-11-4 ]
YieldReaction ConditionsOperation in experiment
61% General procedure: 4-Bromo substituted triphenylamine was dissolved in dry THF under nitrogen atmosphere and it was cooled to -78 C . n-BuLi was added with syringe and kept at -78 C for one hour. 2-Isopropoxy-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane was added dropwise. After addition, the solution was allowed to warm up to room temperature for overnight reaction. After quenching of the reaction with ammonium chloride solution, the water layer was extracted with chloroform and the combined organic layer was dried over MgSO4. After the remove of the solvent under reduced pressure, the residue was purified by silica gel column chromatography (petroleum ether/dichloromethane 1:1) to afford the product as white solids.
  • 2
  • 4,4,5,5-tetramethyl-2-(4,4,5,5-tetramethyl-1,3-dioxolan-2-yl)-1,3,2-dioxaborolane [ No CAS ]
  • [ 100308-69-8 ]
  • [ 1440066-11-4 ]
 

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