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CAS No. : | 1446113-41-2 | MDL No. : | |
Formula : | C7H6N2OS | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 166.20 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Class: | ||
Precautionary Statements: | UN#: | ||
Hazard Statements: | Packing Group: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 5 steps 1.1: trichlorophosphate / N,N-dimethyl-formamide / 4 h / 110 °C 2.1: palladium(II) hydroxide; triethylamine; hydrogen / methanol / 5 h 3.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / benzene / 2 h / 75 °C 4.1: potassium iodide / N,N-dimethyl-formamide / 1 h / 40 °C 4.2: 15 h / 40 °C 5.1: water; sodium hydroxide / tetrahydrofuran / 2 h / 20 °C | ||
Multi-step reaction with 4 steps 1.1: trichlorophosphate; N,N-dimethyl-formamide / 4 h / 110 °C 2.1: palladium(II) hydroxide; triethylamine; hydrogen / methanol / 5 h 3.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / benzene / 2 h / 75 °C 3.2: 1 h / 40 °C 3.3: 15 h / 40 °C 4.1: sodium hydroxide; water / tetrahydrofuran / 2 h / 20 °C |