Home Cart Sign in  
Chemical Structure| 149966-41-6 Chemical Structure| 149966-41-6

Structure of 149966-41-6

Chemical Structure| 149966-41-6

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 149966-41-6 ]

CAS No. :149966-41-6
Formula : C7H8BrNO2
M.W : 218.05
SMILES Code : COC1=CN=C(Br)C(OC)=C1

Safety of [ 149966-41-6 ]

Application In Synthesis of [ 149966-41-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 149966-41-6 ]

[ 149966-41-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 18677-48-0 ]
  • [ 149966-41-6 ]
YieldReaction ConditionsOperation in experiment
70% With N-Bromosuccinimide; In acetonitrile; for 1h;Heating / reflux; To a stirred solution of <strong>[18677-48-0]3,5-dimethoxypyridine</strong> (780 mg, 5.6 mmol) in dry MeCN (24 ml) was added N-bromosuccinimide (1.Og, 5.6 mmol) and the reaction was heated to reflux for 1 hour. After cooling, the solvent was removed under vacuum and the residue was triturated with diethyl ether to precipitate the succinimide by-product and filtered. The filtrate was concentrated onto silica-gel and the residue purified by flash chromatography (silica-gel, eluted with hexanes : EtOAc, 3:1) to afford the product as a white solid (860 mg, 70%). 1H-NMR (300 MHz, CDCl3) delta 7.67 (d, J= 2.5 Hz, IH), 6.71 (d, J= 2.5 Hz, IH), 3.87 (s, 3H), 3.85 (s, 3H).
 

Historical Records