Home Cart Sign in  
Chemical Structure| 150256-18-1 Chemical Structure| 150256-18-1

Structure of 150256-18-1

Chemical Structure| 150256-18-1

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 150256-18-1 ]

CAS No. :150256-18-1
Formula : C13H11BrO2
M.W : 279.13
SMILES Code : O=C(OCC)C1=CC=C2C(Br)=CC=CC2=C1
MDL No. :MFCD18411898

Safety of [ 150256-18-1 ]

Application In Synthesis of [ 150256-18-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 150256-18-1 ]

[ 150256-18-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 64-17-5 ]
  • [ 1013-83-8 ]
  • [ 150256-18-1 ]
YieldReaction ConditionsOperation in experiment
98% With thionyl chloride; at 0 - 80℃; for 5.0h; Synthesis of ethyl 5-bromo-2-naphthoate (2) To a solution of <strong>[1013-83-8]5-bromo-2-naphthoic acid</strong> (1, 2.0 g, 8.0 mmol) in ethanol (50 mL) was added thionyl chloride (5 mL) at 0° C. The reaction mixture was refluxed at 80° C. for 5 h. After completion, the reaction was basified with aqueous saturated sodium bicarbonate solution at 0° C. and diluted with Ethyl acetate. The organic layer was washed with brine, dried over sodium sulfate and concentrated to afford ethyl 5-bromo-2-naphthoate (2) as a white solid. Yield: 2.2 g, 98percent; MS (ESI) m/z 279 [M+1]+.
 

Historical Records