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Chemical Structure| 1529781-98-3 Chemical Structure| 1529781-98-3

Structure of 1529781-98-3

Chemical Structure| 1529781-98-3

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Product Details of [ 1529781-98-3 ]

CAS No. :1529781-98-3
Formula : C8H17NO
M.W : 143.23
SMILES Code : OC1CC(C)(C)CC(N)C1
MDL No. :MFCD24497686

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Application In Synthesis of [ 1529781-98-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1529781-98-3 ]

[ 1529781-98-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 873-95-0 ]
  • [ 1529781-98-3 ]
YieldReaction ConditionsOperation in experiment
With hydrogen; sodium hydroxide; In ethanol; water; at 60℃; under 3750.38 Torr; for 48h; To a solution of 3-amino-5,5-dimethyl-cyclohex-2-enone (2 g, 14.37 mmol) in EtOH (20 mL) and aq. NaOH 20% (0.6 mL) was added Raney-Nickel (1.8 g). The reaction mixture was placed under an hydrogen atmosphere (5 bars) at 60C and stirred for 2 days. Subsequently the reaction mixture was cooled to RT and filtered through Hyllo Super Gel medium with EtOH. The filtrate was concentrated to give the mixture of diastereoisomers directly engaged in the next step without purification. MS (UPLCMS): 144.1 [M+H]+.
 

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