Purity | Size | Price | VIP Price | USA Stock *0-1 Day | Global Stock *5-7 Days | Quantity | |||||
{[ item.p_purity ]} | {[ item.pr_size ]} |
{[ getRatePrice(item.pr_usd, 1,1) ]} {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate) ]} |
{[ getRatePrice(item.pr_usd, 1,1) ]} | Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate) ]} {[ getRatePrice(item.pr_usd,1,item.mem_rate) ]} | {[ item.pr_usastock ]} | Inquiry - | {[ item.pr_chinastock ]} | Inquiry - |
* Storage: {[proInfo.prStorage]}
CAS No. : | 1538579-23-5 | MDL No. : | MFCD31700807 |
Formula : | C14H10O4 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | LXIGMDZIEMIPTI-UHFFFAOYSA-N |
M.W : | 242.23 | Pubchem ID : | 102335525 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P280-P301+P312-P302+P352-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 4 steps 1.1: bromine; acetic acid / 13 h / 0 - 25 °C 2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere 2.2: 1 h / Inert atmosphere 3.1: boron tribromide / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere 4.1: potassium carbonate / tetrahydrofuran / 0.5 h / Reflux 4.2: 72 h / Reflux |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
100% | With acetic acid In tetrahydrofuran at 20℃; for 12h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
100% | With copper(l) iodide; triethylamine; N-ethyl-N,N-diisopropylamine In tetrahydrofuran; water at 70℃; for 72h; Schlenk technique; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 3 steps 1.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere 1.2: 1 h / Inert atmosphere 2.1: boron tribromide / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere 3.1: potassium carbonate / tetrahydrofuran / 0.5 h / Reflux 3.2: 72 h / Reflux |