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Chemical Structure| 15554-15-1 Chemical Structure| 15554-15-1

Structure of 15554-15-1

Chemical Structure| 15554-15-1

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Product Details of [ 15554-15-1 ]

CAS No. :15554-15-1
Formula : C32H17AlN8O
M.W : 556.51
SMILES Code : C1(C([N-]C(C2=CC=CC=C2/3)=NC3=N/4)=N/5)=CC=CC=C1C5=N\C(C6=CC=CC=C6/7)=NC7=N/C8=C9C=CC=CC9=C4[N-]8.[Al+3].[OH-]
MDL No. :MFCD00274640

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Application In Synthesis of [ 15554-15-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 15554-15-1 ]

[ 15554-15-1 ] Synthesis Path-Downstream   1~3

  • 2
  • [ 14154-42-8 ]
  • [ 7664-93-9 ]
  • [ 15554-15-1 ]
YieldReaction ConditionsOperation in experiment
at 20 - 40℃; for 3h; Subsequently, 100 parts of <strong>[14154-42-8]chloroaluminum phthalocyanine</strong> was slowly added to 1,200 parts of concentrated sulfuric acid at room temperature in a reaction vessel. After stirring at 40 C for 3 hours, a sulfuric acid solution was poured into 24000 parts of cold water at 3 C. The blue precipitate was filtered, washed with water and dried to obtain 92 parts of a compound represented by the following general formula (2) Thereby obtaining a phthalocyanine compound (PB-1).
  • 3
  • [ 14154-42-8 ]
  • [ 7732-18-5 ]
  • [ 15554-15-1 ]
YieldReaction ConditionsOperation in experiment
With sodium hydroxide; In acetone; at 50℃; for 4h; Example 2: Synthesis of Hydroxy Aluminum Phthalocyanine20 g (0.34 mol) of the aluminum chloride phthalocyanine compound of Example 1,200 ml of acetone and 20 ml of distilled water were added to a 1 liter three-necked round bottom flask, followed by stirring.It is hydrolyzed at 50 C. for 4 hours with sodium hydroxide as a catalyst and filtered.After filtration, wash the wet cake with distilled water until the filtrate is neutral. Then, the obtained wet cake was dried in an oven dryer to obtain hydroxy aluminum phthalocyanine.The elemental analysis and ICP measurement results of the compound thus obtained are shown in Table 2 below, and the overall purity was analyzed to be 99.15%.
 

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