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Chemical Structure| 15676-11-6 Chemical Structure| 15676-11-6

Structure of 15676-11-6

Chemical Structure| 15676-11-6

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Product Details of [ 15676-11-6 ]

CAS No. :15676-11-6
Formula : C9H10N2O2
M.W : 178.19
SMILES Code : O=C(OC)C1=CC=CC(C(N)=N)=C1

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Application In Synthesis of [ 15676-11-6 ]

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  • Downstream synthetic route of [ 15676-11-6 ]

[ 15676-11-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 13531-48-1 ]
  • [ 15676-11-6 ]
YieldReaction ConditionsOperation in experiment
61 g With hydroxylamine; In ethanol; water; at 100℃; for 1h; 50 g of <strong>[13531-48-1]methyl 3-cyanobenzoate</strong> was dissolved in 500 ml of ethanol,To this was added 41 ml of 50percent aqueous hydroxylamine (620 mmol).The reaction mixture was stirred at 100 ° C for 1 hour and the solvent was removed under reduced pressure.The oily residue was dissolved in 100 ml of 20/80 ethanol / toluene,Re-concentrate. 61 g of 3- (carbamimidoyl) -benzoic acid methyl ester was obtained.
 

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