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Chemical Structure| 16119-99-6 Chemical Structure| 16119-99-6

Structure of 16119-99-6

Chemical Structure| 16119-99-6

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Product Details of [ 16119-99-6 ]

CAS No. :16119-99-6
Formula : C4H3Cl2N3
M.W : 163.99
SMILES Code : CC1=C(Cl)N=C(Cl)N=N1
MDL No. :MFCD28642053

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Application In Synthesis of [ 16119-99-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 16119-99-6 ]

[ 16119-99-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 932-53-6 ]
  • [ 16119-99-6 ]
YieldReaction ConditionsOperation in experiment
With trichlorophosphate; at 110℃; for 4h; To a solution of <strong>[932-53-6]6-methyl-1,2,4-triazine-3,5(2H,4H)-dione</strong> 1 (600 mg, 4.7 mmol) in POCl3 (50 mL). The reaction mixture was stirred at 110 C. for 4 hours. The reaction mixture was concentrated under vacuum to get crude 3,5-dichloro-6-methyl-1,2,4-triazine2 (650 mg, 84%), which was used for the next step directly. LRMS (M+H+) m/z: calcd 163.97; found 164.
 

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