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Chemical Structure| 161462-33-5 Chemical Structure| 161462-33-5

Structure of 161462-33-5

Chemical Structure| 161462-33-5

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Product Details of [ 161462-33-5 ]

CAS No. :161462-33-5
Formula : C9H6F3NS
M.W : 217.21
SMILES Code : FC(C1=CC=C(C#N)C(SC)=C1)(F)F

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Application In Synthesis of [ 161462-33-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 161462-33-5 ]

[ 161462-33-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1813-33-8 ]
  • [ 5188-07-8 ]
  • [ 161462-33-5 ]
YieldReaction ConditionsOperation in experiment
With tetrabutyl-ammonium chloride; In 5,5-dimethyl-1,3-cyclohexadiene; at 50 - 60℃; Add a certain amount of xylene to the reactor,Sodium thiomethoxide,Intermediate 1 and catalyst tetrabutylammonium chloride,Warm up to 5060C,Insulation 2~3hSampling qualifiedAfter the static separationSodium thiomethoxideThen add a fixed amount of water for washing.After washing, separate the liquid,Organic phase negative pressure recovery of xylene applied,Intermediate 2 is obtained.Among them, the intermediate 1 is C9H6F3NS, the product is C9H6F3NS and sodium chloride NaCl; the mass ratio of C9H6F3NS and sodium chloride NaCl is 434:17.
 

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