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Chemical Structure| 162100-44-9 Chemical Structure| 162100-44-9

Structure of 162100-44-9

Chemical Structure| 162100-44-9

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Product Details of [ 162100-44-9 ]

CAS No. :162100-44-9
Formula : C9H10ClN
M.W : 167.64
SMILES Code : CC1=CC2=C(NCC2)C=C1Cl
MDL No. :MFCD09907618
InChI Key :ZAMJLADJGLXVOJ-UHFFFAOYSA-N
Pubchem ID :22186080

Safety of [ 162100-44-9 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 162100-44-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 162100-44-9 ]

[ 162100-44-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 162100-42-7 ]
  • [ 162100-44-9 ]
YieldReaction ConditionsOperation in experiment
3.5 g With sodium cyanoborohydride; acetic acid; at 20.0℃; for 1.0h;Inert atmosphere; Industrial scale; To a solution of Compound D (3.5 g, 21 mmol) in AcOH (40 mL) was added sodium cyanoborohydride (2.7 g, 43 mmol) and the mixture was purged with N2 for 1 h at room temperature.The reaction was complete by TLC (PE / EA = 10/1), further ethyl acetate EA (200 ml) was added and the mixture was made basic with a 5N NaOH solution (200 ml) at a pH of about 8. The organic layer was separated, Wash once, fullAnd brine once, dried over anhydrous sodium sulfate, dried to give 3.5g of brown solid Compound E, spare. Yield 98%.
 

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