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[ CAS No. 162662-27-3 ]

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Chemical Structure| 162662-27-3
Chemical Structure| 162662-27-3
Structure of 162662-27-3 * Storage: {[proInfo.prStorage]}

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Product Details of [ 162662-27-3 ]

CAS No. :162662-27-3 MDL No. :MFCD03412067
Formula : C8H11BO4 Boiling Point : 346.27°C at 760 mmHg
Linear Structure Formula :- InChI Key :N/A
M.W :181.98 g/mol Pubchem ID :-
Synonyms :

Safety of [ 162662-27-3 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P233-P260-P261-P264-P271-P280-P302+P352-P304-P304+P340-P305+P351+P338-P312-P321-P332+P313-P337+P313-P340-P362-P403-P403+P233-P405-P501 UN#:N/A
Hazard Statements:H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 162662-27-3 ]

  • Downstream synthetic route of [ 162662-27-3 ]

[ 162662-27-3 ] Synthesis Path-Downstream   1~15

  • 1
  • [ 64648-81-3 ]
  • [ 162662-27-3 ]
  • [ 132113-71-4 ]
YieldReaction ConditionsOperation in experiment
83% With sodium carbonate In toluene
83% With sodium carbonate In toluene
  • 2
  • [ 162662-27-3 ]
  • 5-Bromo-4,7-dimethoxyindole-2-carboxylic acid methyl ester [ No CAS ]
  • 4,7-Dimethoxy-5-(4-methoxymethoxy-phenyl)-1H-indole-2-carboxylic acid methyl ester [ No CAS ]
YieldReaction ConditionsOperation in experiment
78% With sodium carbonate In toluene
  • 3
  • [ 201230-82-2 ]
  • [ 162662-27-3 ]
  • [ 162662-26-2 ]
  • 11-(Dimethylamino)-2-<4'-<(methoxymethyl)oxy>phenyl>-12-<<2''-(trimethylsilyl)ethoxy>methyl>-9H-imidazo<4',5':3,4>pyrido<2,3-b>indole [ No CAS ]
  • [ 162662-28-4 ]
YieldReaction ConditionsOperation in experiment
1: 58% 2: 19% With potassium carbonate; lithium chloride In various solvent(s) at 80℃; for 3h;
  • 4
  • [ 162662-27-3 ]
  • [ 162662-26-2 ]
  • 11-(Dimethylamino)-2-<4'-<(methoxymethyl)oxy>phenyl>-12-<<2''-(trimethylsilyl)ethoxy>methyl>-9H-imidazo<4',5':3,4>pyrido<2,3-b>indole [ No CAS ]
  • [ 162662-28-4 ]
YieldReaction ConditionsOperation in experiment
1: 19% 2: 58% With carbon monoxide; potassium carbonate; lithium chloride In various solvent(s) at 80℃; for 3h;
  • 5
  • [ 162662-27-3 ]
  • [ 402490-59-9 ]
  • [ 402490-66-8 ]
YieldReaction ConditionsOperation in experiment
83% With tetrabutyl ammonium fluoride; triphenylphosphine In tetrahydrofuran for 5h; Heating;
  • 6
  • [ 162662-27-3 ]
  • [ 402490-61-3 ]
  • [ 402490-67-9 ]
YieldReaction ConditionsOperation in experiment
71% With tetrabutyl ammonium fluoride; triphenylphosphine In tetrahydrofuran for 5h; Heating;
> 95 % de With bis-triphenylphosphine-palladium(II) chloride; tetrabutyl ammonium fluoride; triphenylphosphine In tetrahydrofuran
  • 7
  • [ 162662-27-3 ]
  • [ 216485-72-2 ]
  • (1-ethyl-5-hydroxy-1<i>H</i>-pyrazol-4-yl)-(6-methanesulfonyl-4'-methoxymethoxy-2-methyl-biphenyl-3-yl)-methanone [ No CAS ]
YieldReaction ConditionsOperation in experiment
With potassium carbonate In water; acetonitrile Heating;
  • 8
  • [ 162662-27-3 ]
  • [ 216485-70-0 ]
  • 1-(1,1-dimethylethyl)-5-hydroxy-4-(3-(4-(methoxymethoxy)phenyl)-2-methyl-4-(methylsulfonyl)benzoyl)pyrazole [ No CAS ]
YieldReaction ConditionsOperation in experiment
77% With potassium carbonate In water; acetonitrile for 1h; Heating;
  • 9
  • [ 25458-45-1 ]
  • [ 162662-27-3 ]
YieldReaction ConditionsOperation in experiment
71% Stage #1: p-methoxymethoxybromobenzene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Stage #2: With Triisopropyl borate In tetrahydrofuran; hexane at -78 - 20℃; for 5h; Stage #3: With hydrogenchloride In tetrahydrofuran; hexane; water at 0℃; for 0.5h;
71% Stage #1: p-methoxymethoxybromobenzene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Stage #2: With Triisopropyl borate In tetrahydrofuran; hexane at -78 - 20℃; for 5h; Stage #3: With hydrogenchloride In tetrahydrofuran; hexane at 0℃; for 0.5h;
15.b 4-(Methoxymethoxy-2'-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthyl)-[1,1';4',1"terphenyl-4"-carboxylic Acid (b) 4-Methoxymethoxyphenylboronic Acid. In a manner similar to that of Example 1(a), starting with 63.81 g (293.0 mmol) of 4-methoxymethoxybromobenzene, 35.42 g (80%) of the expected product are obtained in the form of a white solid with a melting point of 122° C. 1H NMR (CDCl3) δ 3.52 (s, 3H), 5.27 (s, 2H), 7.15 (d, 2H, J=8.6 Hz), 8.16 (d, 2H, J=8.6 Hz).
28.b (b) (b) 4-Methoxymethoxybenzeneboronic acid: In a similar manner to that of Example 2(a), starting with 63.81 g (293.0 mmol) of 4-methoxymethoxybromobenzene obtained in Example 28(a), 35.42 g (80%) of the expected compound are obtained in the form of a white powder with a melting point of 122° C. 1 H NMR (CDCl3) δ 3.52 (s, 3H), 5.27 (s, 2H), 7.14 (d, 2H, J=8.6 Hz), 8.16 (d, 2H, J=8.6 Hz).

  • 10
  • [ 788824-50-0 ]
  • [ 162662-27-3 ]
  • tert-butyl 4-(4'-methoxymethoxyphenoxy)-3-iodophenethylcarbamate [ No CAS ]
YieldReaction ConditionsOperation in experiment
48% With pyridine; copper diacetate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃;
  • 11
  • [ 884320-52-9 ]
  • [ 162662-27-3 ]
  • [ 884320-53-0 ]
YieldReaction ConditionsOperation in experiment
73% With pyridine; copper diacetate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃;
  • 12
  • [ 162662-27-3 ]
  • [ 352469-17-1 ]
  • [ 884320-55-2 ]
YieldReaction ConditionsOperation in experiment
32% With pyridine; copper diacetate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃;
  • 13
  • [ 676498-62-7 ]
  • [ 162662-27-3 ]
  • [ 878050-01-2 ]
YieldReaction ConditionsOperation in experiment
69% With pyridine; copper diacetate; triethylamine In dichloromethane at 20℃;
  • 14
  • [ 106-41-2 ]
  • [ 162662-27-3 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1.1: NaH / dimethylformamide / 20 °C 1.2: 92 percent / dimethylformamide / 0.5 h / 20 °C 2.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C 2.2: triisopropyl borate / tetrahydrofuran; hexane / 5 h / -78 - 20 °C 2.3: 71 percent / aq. HCl / tetrahydrofuran; hexane / 0.5 h / 0 °C
Multi-step reaction with 2 steps 1.1: 92 percent / sodium hydride / dimethylformamide / 0.5 h / 20 °C 2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C 2.2: triisopropyl borate / tetrahydrofuran; hexane / 5 h / -78 - 20 °C 2.3: 71 percent / HCl / tetrahydrofuran; hexane; H2O / 0.5 h / 0 °C
  • 15
  • [ 162662-27-3 ]
  • 4-[4-(2-amino-ethyl)-2-methyl-phenoxy]-phenol [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 69 percent / Cu(OAc)2; Et3N; pyridine / 4 Angstroem molecular sieves / CH2Cl2 / 20 °C 2: 96 percent / HCl / ethyl acetate / 20 °C
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