Alternatived Products of [ 16528-77-1 ]
Product Details of [ 16528-77-1 ]
CAS No. : | 16528-77-1 |
MDL No. : | MFCD00224838 |
Formula : |
C22H45NO
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Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
339.60
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Pubchem ID : | - |
Synonyms : |
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Application In Synthesis of [ 16528-77-1 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 16528-77-1 ]
- 1
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[ 110-91-8 ]
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[ 629-93-6 ]
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[ 16528-77-1 ]
Yield | Reaction Conditions | Operation in experiment |
|
at 140℃; |
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- 2
-
[ 110-91-8 ]
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[ 112-89-0 ]
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[ 16528-77-1 ]
Yield | Reaction Conditions | Operation in experiment |
|
at 140℃; |
|
- 3
-
[ 16528-77-1 ]
-
[ 77-78-1 ]
-
[ 3050-84-8 ]
- 4
-
[ 111-44-4 ]
-
[ 124-30-1 ]
-
[ 16528-77-1 ]
- 5
-
[ 5299-54-7 ]
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[ 16528-77-1 ]
Yield | Reaction Conditions | Operation in experiment |
|
With lithium aluminium tetrahydride In diethyl ether 1) 0-5 deg C, 30 min, 2) room temperature, 2 h; Yield given; |
|
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With lithium aluminium tetrahydride; sulfuric acid In tetrahydrofuran at 0℃; |
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Reference:
[1]Oesch, Urs; Brzozka, Zbigniew; Xu, Aiping; Rusterholz, Bruno; Suter, Gabriela; et al.
[Analytical Chemistry, 1986, vol. 58, # 11, p. 2285 - 2289]
[2]Kiuchi; Nishizawa; Kawanishi; Kinoshita; Ohsima; Uchitani; Sekino; Ishida; Kondo; Tsuda
[Chemical and Pharmaceutical Bulletin, 1992, vol. 40, # 12, p. 3234 - 3244]
Yield | Reaction Conditions | Operation in experiment |
|
Cumolhydroperoxid, E., MoO2-acetylacetonat, zuletzt 60grad -> entspr. Aminoxid 3d; |
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- 7
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[ 112-76-5 ]
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[ 16528-77-1 ]
Yield | Reaction Conditions | Operation in experiment |
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Multi-step reaction with 2 steps
1: (C2H5)3N / tetrahydrofuran / 1 h / 0 °C
2: LiAlH4 / diethyl ether / 1) 0-5 deg C, 30 min, 2) room temperature, 2 h |
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- 8
-
[ 16528-77-1 ]
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[ 117950-12-6 ]
Yield | Reaction Conditions | Operation in experiment |
|
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IX EXAMPLE IX
EXAMPLE IX The process of Example I is repeated except that the amine used is N-octadecyl-morpholine. The yield of N-octadecyl-N-[(2-pyrrolidonyl)methyl] morpholinium chloride is quantitative. |