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[ CAS No. 178261-41-1 ] {[proInfo.proName]}

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Chemical Structure| 178261-41-1
Chemical Structure| 178261-41-1
Structure of 178261-41-1 * Storage: {[proInfo.prStorage]}
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Product Details of [ 178261-41-1 ]

CAS No. :178261-41-1 MDL No. :MFCD04108105
Formula : C13H18N2O2S Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W :266.36 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 178261-41-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 178261-41-1 ]

[ 178261-41-1 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 47173-80-8 ]
  • [ 178261-41-1 ]
  • [ 180465-66-1 ]
YieldReaction ConditionsOperation in experiment
67% With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20℃; N-Boc-OBn-D-Serine (0.69 g, 2. 34mmol) was added to a solution of C (0.57 g, 2. 13mmol), 1- (3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride (0.45 g, 2.34mmol) and 1-hydroxybenzotriazole (0.32 g, 2. 34mmol) in dichloromethane (5 mL) and the resulting solution was stirred overnight at room temperature. The reaction was then washed with a saturated solution of citric acid (5 mL) and then a saturated solution of NaHC03 (5 mL), dried over Na2S04, filtered and evaporated in vacuo. The product was purified by silica gel chromatography eluting with ethyl acetate/cyclohexane (1/1) to give 0.77g (67%) of D as a white solid.
  • 3
  • [ 122860-33-7 ]
  • [ 178261-41-1 ]
  • 4
  • [ 24686-78-0 ]
  • [ 178261-41-1 ]
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