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Chemical Structure| 17945-49-2 Chemical Structure| 17945-49-2

Structure of 17945-49-2

Chemical Structure| 17945-49-2

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Product Details of [ 17945-49-2 ]

CAS No. :17945-49-2
Formula : C6H15NO
M.W : 117.19
SMILES Code : CC(NC)(C)CCO
MDL No. :MFCD19223048

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Application In Synthesis of [ 17945-49-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 17945-49-2 ]

[ 17945-49-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 130985-42-1 ]
  • [ 17945-49-2 ]
YieldReaction ConditionsOperation in experiment
6.45 g With lithium aluminium tetrahydride; In tetrahydrofuran;Reflux; To a solution of ethyl 3-((tert-butoxycarbonyl) amino)-3-methylbutanoate (13.5 g, 55.0 mmol) in THF (100 mL) was added L1AIH4 solution (2.0 M, 83 mL) dropwise at 0 C. Then the reaction mixture was refluxed overnight, cooled to r.t, quenched by addition of water (4.5 mL), filtrated, and concentrated to afford the title compound (6.45 g). LC-MS (ESI): m/z 1 18 [M+l ]+; 0.35 min (ret time).
 

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