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[ CAS No. 184289-85-8 ] {[proInfo.proName]}

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Chemical Structure| 184289-85-8
Chemical Structure| 184289-85-8
Structure of 184289-85-8 * Storage: {[proInfo.prStorage]}
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Product Details of [ 184289-85-8 ]

CAS No. :184289-85-8 MDL No. :MFCD22124870
Formula : C20H20N2O2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W :320.39 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 184289-85-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 184289-85-8 ]

[ 184289-85-8 ] Synthesis Path-Downstream   1~4

  • 2
  • [ 184289-85-8 ]
  • [ 159634-47-6 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 7 steps 1: NaBH4 / toluene / 0.5 h / -2 °C 2: DIEA / tetrahydrofuran / 2 h / 5 - 8 °C 3: 93 percent / H2 / Pd-C / ethanol / 5 h / 65 °C / 2068.6 Torr 4: DCC, HOBt / H2O; various solvent(s) / 5 h / Ambient temperature 5: MsOH / ethanol / 7.5 h / 35 - 40 °C 6: DCC, HOBt / various solvent(s) / 2 h / Ambient temperature 7: MsOH / ethanol / 35 - 40 °C
  • 3
  • [ 184289-85-8 ]
  • [ 159752-10-0 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 8 steps 1: NaBH4 / toluene / 0.5 h / -2 °C 2: DIEA / tetrahydrofuran / 2 h / 5 - 8 °C 3: 93 percent / H2 / Pd-C / ethanol / 5 h / 65 °C / 2068.6 Torr 4: DCC, HOBt / H2O; various solvent(s) / 5 h / Ambient temperature 5: MsOH / ethanol / 7.5 h / 35 - 40 °C 6: DCC, HOBt / various solvent(s) / 2 h / Ambient temperature 7: MsOH / ethanol / 35 - 40 °C 8: ethanol; ethyl acetate / 55 °C
Multi-step reaction with 6 steps 1: sodium tetrahydroborate / methanol 2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran 3: palladium 10% on activated carbon; hydrogen / ethanol 4: benzotriazol-1-ol; dicyclohexyl-carbodiimide / Isopropyl acetate; water 5: benzotriazol-1-ol; dicyclohexyl-carbodiimide / Isopropyl acetate; water 6: ethanol
  • 4
  • [ 7188-38-7 ]
  • [ 480-63-7 ]
  • [ 184289-85-8 ]
  • C35H41N3O4 [ No CAS ]
YieldReaction ConditionsOperation in experiment
70% In dichloromethane; at 20℃; for 24h; General procedure: Indolenine 3 (1 equiv) was dissolved in CH2Cl2 (1 M) followed bythe addition of the corresponding acid (1.05 equiv) and isocyanide(1.05 equiv). The reaction mixture was stirred for 24 h at r.t. Afterwards, CH2Cl2 was evaporated under vacuum to achievethe crude residue that was subjected to column chromatography(SiO2, CH2Cl2-EtOAc = 4:1)
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