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CAS No. : | 18706-27-9 | MDL No. : | MFCD11855862 |
Formula : | C11H7BrF3N | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 290.08 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Class: | ||
Precautionary Statements: | UN#: | ||
Hazard Statements: | Packing Group: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
77% | With n-butyllithium In tetrahydrofuran; hexane at -75℃; for 0.75h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
74% | With n-butyllithium; diisopropylamine In tetrahydrofuran; hexane at -75℃; for 2h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
87% | With phosphorus(V) oxybromide at 150℃; for 2h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
74% | With n-butyllithium In tetrahydrofuran; hexane at -75℃; for 0.25h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: 62 percent / polyphosphoric acid / 2 h / 150 °C 2: 87 percent / phosphorus oxybromide / 2 h / 150 °C |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: 74 percent / butyllithium; diisopropylamine / tetrahydrofuran; hexane / 2 h / -75 °C 2: 68 percent / butyllithium / hexane / 6 h / -75 °C |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: 74 percent / butyllithium; diisopropylamine / tetrahydrofuran; hexane / 2 h / -75 °C 2: 89 percent / potassium carbonate / acetone / 6 h / 25 °C |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 4 steps 1: 74 percent / butyllithium; diisopropylamine / tetrahydrofuran; hexane / 2 h / -75 °C 2: 89 percent / potassium carbonate / acetone / 6 h / 25 °C 3: 82 percent / tributyltin hydride; azoisobutyronitrile / tetrahydrofuran / 20 h / 75 °C 4: sodium hydroxide / H2O; methanol / 6 h / 50 °C |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 3 steps 1: 74 percent / butyllithium; diisopropylamine / tetrahydrofuran; hexane / 2 h / -75 °C 2: 89 percent / potassium carbonate / acetone / 6 h / 25 °C 3: 82 percent / tributyltin hydride; azoisobutyronitrile / tetrahydrofuran / 20 h / 75 °C |