Home Cart Sign in  
Chemical Structure| 115-84-4 Chemical Structure| 115-84-4
Chemical Structure| 115-84-4

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of 2-Butyl-2-ethyl-1,3-propanediol

CAS No. :115-84-4
Formula : C9H20O2
M.W : 160.25
SMILES Code : OCC(CC)(CCCC)CO
MDL No. :MFCD00004697
InChI Key :DSKYSDCYIODJPC-UHFFFAOYSA-N
Pubchem ID :61038

Safety of 2-Butyl-2-ethyl-1,3-propanediol

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H319
Precautionary Statements:P305+P351+P338

Application In Synthesis of 2-Butyl-2-ethyl-1,3-propanediol

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 115-84-4 ]

[ 115-84-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 51792-34-8 ]
  • [ 115-84-4 ]
  • 3-butyl-3-ethyl-3,4-dihydro-2H-thieno[3,4-b][1,4]dioxepine [ No CAS ]
YieldReaction ConditionsOperation in experiment
80% With toluene-4-sulfonic acid; In toluene; at 110℃; for 24h; As shown in Scheme 4 below, To 100 mL of toluene in which 5.28 g (27.7 mmol) of p-toluenesulfonic acid (p-TSA) was dissolved,20.0 g (138.7 mmol) of <strong>[51792-34-8]3,4-dimethoxythiophene</strong> (compound (1)), and 88.9 g (554.8 mmol) of 2-butyl-2-ethyl-1,3-propanediol, compound (6) the reaction was carried out with stirring at 110 DEG C for 24 hours. After completion of the reaction,To the reaction was added a mixed solvent of water and ethyl acetate (EtOAc), The product was extracted into an organic layer,Washed with brine,The water was removed using anhydrous Na2SO4, followed by filtration and concentration.The product was separated by column chromatography on SiO2 (eluent: hexane: ethyl acetate = 10: 1 as a mixture)3-ethyl-3,4-dihydro-2H-thieno [3,4-b] [1,4] [3,4-b] [1,4] dioxepine,21.7 to 26.7 g of compound (7)) (yield: 65-80percent). 1H-NMR data of the obtained compound are as follows: 1H-NMR (CDCl3, Varian 400 MHz): delta 0.86-0.94 (6H, m), 1.21-1.48 (8H, m), 3.85 (4H, s),6.42 (2H, s).
 

Historical Records

Technical Information

Categories