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Chemical Structure| 205180-02-5 Chemical Structure| 205180-02-5

Structure of 205180-02-5

Chemical Structure| 205180-02-5

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Product Details of [ 205180-02-5 ]

CAS No. :205180-02-5
Formula : C14H19NO2
M.W : 233.31
SMILES Code : O=C(OC1CCCC1)[C@@H](N)CC2=CC=CC=C2
MDL No. :MFCD13329536

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Application In Synthesis of [ 205180-02-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 205180-02-5 ]

[ 205180-02-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 205180-02-5 ]
  • [ 156866-52-3 ]
  • [ 914606-08-9 ]
YieldReaction ConditionsOperation in experiment
<strong>[156866-52-3](4-Formyl-benzyl)-carbamic acid tert-butyl ester</strong> (200 mg, 0.85 mmol) was dissolved in DCE (10 ml_) and to this was added phenyl alanine cyclopentyl ester (214 mg, 0.94 mmol). The reaction was stirred at r.t. for 15 min. Sodium triacetoxyborohydride (538 mg, 2.55 mmol) and acetic acid (60 uL) were added and the reaction stirred for a further 1 h. Saturated sodium bicarbonate (10 ml) was added and the solution diluted with DCM (20 ml_). The organic layer was isolated and concentrated to afford the desired product which was taken onto the next step without further purification, m/z 453 [M++H+
 

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